Benzoic acid, 4-[3-[[(1,1-dimethylethoxy)carbonyl]amino]propoxy]-3-[3-(1-methylethen yl)-4-quinolinyl]-, 3-[[(1,1-dimethylethoxy)carbonyl]amino]propyl ester

Base Information

Chemical Name:Benzoic acid, 4-[3-[[(1,1-dimethylethoxy)carbonyl]amino]propoxy]-3-[3-(1-methylethen yl)-4-quinolinyl]-, 3-[[(1,1-dimethylethoxy)carbonyl]amino]propyl ester
CAS No.:491602-11-0
Molecular Formula:C35H45N3O7
Molecular Weight:619.758
Hs Code.:

Benzoic acid,
4-[3-[[(1,1-dimethylethoxy)carbonyl]amino]propoxy]-3-[3-(1-methylethen
yl)-4-quinolinyl]-, 3-[[(1,1-dimethylethoxy)carbonyl]amino]propyl ester

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Chemical Property of Benzoic acid, 4-[3-[[(1,1-dimethylethoxy)carbonyl]amino]propoxy]-3-[3-(1-methylethen yl)-4-quinolinyl]-, 3-[[(1,1-dimethylethoxy)carbonyl]amino]propyl ester

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Technology Process of Benzoic acid, 4-[3-[[(1,1-dimethylethoxy)carbonyl]amino]propoxy]-3-[3-(1-methylethen yl)-4-quinolinyl]-, 3-[[(1,1-dimethylethoxy)carbonyl]amino]propyl ester

There total 3 articles about Benzoic acid, 4-[3-[[(1,1-dimethylethoxy)carbonyl]amino]propoxy]-3-[3-(1-methylethen yl)-4-quinolinyl]-, 3-[[(1,1-dimethylethoxy)carbonyl]amino]propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 83948-53-2
3-bromopropylamine tert-butylcarbamate

: 491602-10-9
4-hydroxy-3-(3-isopropenyl-quinolin-4-yl)-benzoic acid

: 491602-11-0
4-(3-tert-butoxycarbonylamino-propoxy)-3-(3-isopropenyl-quinolin-4-yl)-benzoic acid 3-tert-butoxycarbonylamino-propyl ester

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 20h;
DOI:10.1021/ol049100q

Reference yield:

: 741731-30-6
(2R,3R,4R)-3-Chloro-5-guanidino-4-hydroxy-2-[4-hydroxy-3-(3-isopropenyl-quinolin-4-yl)-benzoylamino]-pentanoic acid

: 491602-11-0
4-(3-tert-butoxycarbonylamino-propoxy)-3-(3-isopropenyl-quinolin-4-yl)-benzoic acid 3-tert-butoxycarbonylamino-propyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: NaOH / H₂O / 48 h / Heating

2: 91 percent / K₂CO₃ / dimethylformamide / 20 h / 50 °C

With sodium hydroxide; potassium carbonate; In water; N,N-dimethyl-formamide;
DOI:10.1021/ol049100q

Reference yield:

: FR₂₂₅₆₅₉

: 491602-11-0
4-(3-tert-butoxycarbonylamino-propoxy)-3-(3-isopropenyl-quinolin-4-yl)-benzoic acid 3-tert-butoxycarbonylamino-propyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: aq. NaOH / 48 h / 20 °C

2: NaOH / H₂O / 48 h / Heating

3: 91 percent / K₂CO₃ / dimethylformamide / 20 h / 50 °C

With sodium hydroxide; potassium carbonate; In water; N,N-dimethyl-formamide;
DOI:10.1021/ol049100q