methyl (2E)-3-(anthracen-9-yl)prop-2-enoate

Base Information

Chemical Name:methyl (2E)-3-(anthracen-9-yl)prop-2-enoate
CAS No.:22844-33-3
Molecular Formula:C₁₈H₁₄O₂
Molecular Weight:262.308
Hs Code.:
NSC Number:382140
Nikkaji Number:J1.003.275J,J701.843F
Mol file:22844-33-3.mol

Synonyms:methyl (2E)-3-(anthracen-9-yl)prop-2-enoate;22844-33-3;methyl (E)-3-anthracen-9-ylprop-2-enoate;NSC382140;Methyl 3-(anthracen-9-yl)acrylate;STK368188;AKOS005445193;AS-0405;NSC-382140;3-(9-Anthryl)acrylic acid methyl ester;(E)-3-(9-Anthracenyl)propenoic acid methyl ester;J-650108

Suppliers and Price of methyl (2E)-3-(anthracen-9-yl)prop-2-enoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of methyl (2E)-3-(anthracen-9-yl)prop-2-enoate

Chemical Property:

Vapor Pressure:1.93E-08mmHg at 25°C
Boiling Point:454.3°C at 760 mmHg
Flash Point:307.9°C
Density:1.199g/cm³
XLogP3:4.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:262.099379685
Heavy Atom Count:20
Complexity:352

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC(=O)C=CC1=C2C=CC=CC2=CC3=CC=CC=C31
Isomeric SMILES:COC(=O)/C=C/C1=C2C=CC=CC2=CC3=CC=CC=C31

Technology Process of methyl (2E)-3-(anthracen-9-yl)prop-2-enoate

There total 10 articles about methyl (2E)-3-(anthracen-9-yl)prop-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 5927-18-4
trimethyl phosphonoacetate

: 642-31-9
9-anthracene aldehyde

: 22844-33-3,101736-45-2
(E)-methyl 3-(anthracen-9-yl)acrylate

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; for 0.5h; Ambient temperature;
DOI:10.1080/00397919808005934

Reference yield: 70.0%

: 5927-18-4
trimethyl phosphonoacetate

: 642-31-9
9-anthracene aldehyde

: 22844-33-3,101736-45-2
(E)-methyl 3-(anthracen-9-yl)acrylate

: 172098-30-5
(Z)-3-Anthracen-9-yl-acrylic acid methyl ester

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; for 0.5h; Ambient temperature;
DOI:10.1021/jo00129a043

Reference yield:

: 642-31-9
9-anthracene aldehyde

: 22844-33-3,101736-45-2
(E)-methyl 3-(anthracen-9-yl)acrylate

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / dimethylformamide / 0.5 h / Ambient temperature

2: benzene / 1 h / Irradiation; various sensitizers; other solvents

With sodium hydride; In N,N-dimethyl-formamide; benzene;
DOI:10.1021/jo00129a043