Ethanone, 2-(3,4-dimethoxyphenyl)-1-(4-methoxyphenyl)-

Base Information

Chemical Name:Ethanone, 2-(3,4-dimethoxyphenyl)-1-(4-methoxyphenyl)-
CAS No.:4927-53-1
Molecular Formula:C17H18O4
Molecular Weight:286.328
Hs Code.:
Mol file:4927-53-1.mol

Synonyms:3',4,4'-Trimethoxy-desoxybenzoin;3,4-dimethoxybenzyl 4-methoxyphenyl ketone;4,3',4'-trimethoxy-deoxybenzoin;2-(3,4-dimethoxyphenyl)-4'-methoxyacetophenone;4,3',4'-Trimethoxy-desoxybenzoin;

Suppliers and Price of Ethanone, 2-(3,4-dimethoxyphenyl)-1-(4-methoxyphenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Ethanone, 2-(3,4-dimethoxyphenyl)-1-(4-methoxyphenyl)-

Chemical Property:

PSA：44.76000
LogP:3.13780

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Ethanone, 2-(3,4-dimethoxyphenyl)-1-(4-methoxyphenyl)-

There total 3 articles about Ethanone, 2-(3,4-dimethoxyphenyl)-1-(4-methoxyphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 10313-60-7
3,4-dimethoxyphenylacetyl chloride

: 100-66-3
methoxybenzene

: 4927-53-1
1'-(3,4-dimethoxyphenyl)-2'-(4''-methoxyphenyl)ethan-2'-one

Guidance literature:: With aluminum (III) chloride; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1021/jacs.1c08615

Reference yield: 79.0%

: 93-40-3
(3,4-Dimethoxyphenyl)acetic acid

: 100-66-3
methoxybenzene

: 4927-53-1
1'-(3,4-dimethoxyphenyl)-2'-(4''-methoxyphenyl)ethan-2'-one

Guidance literature:: With trifluoromethylsulfonic anhydride; In dichloromethane; Cooling with ice;
DOI:10.1016/j.tet.2018.04.017

Reference yield:

: 93-40-3
(3,4-Dimethoxyphenyl)acetic acid

: 4927-53-1
1'-(3,4-dimethoxyphenyl)-2'-(4''-methoxyphenyl)ethan-2'-one

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 3 h / 85 °C / Reflux

2: aluminum (III) chloride / dichloromethane / 2 h / 20 °C

With aluminum (III) chloride; thionyl chloride; In dichloromethane;
DOI:10.1021/jacs.1c08615