Benzenamine, N-[2-(diphenylphosphino)cyclopentylidene]-2,6-bis(1-methylethyl)-

Base Information

Chemical Name:Benzenamine, N-[2-(diphenylphosphino)cyclopentylidene]-2,6-bis(1-methylethyl)-
CAS No.:494191-96-7
Molecular Formula:C₂₉H₃₄NP
Molecular Weight:427.569
Hs Code.:

Synonyms:

Suppliers and Price of Benzenamine, N-[2-(diphenylphosphino)cyclopentylidene]-2,6-bis(1-methylethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Benzenamine, N-[2-(diphenylphosphino)cyclopentylidene]-2,6-bis(1-methylethyl)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Benzenamine, N-[2-(diphenylphosphino)cyclopentylidene]-2,6-bis(1-methylethyl)-

There total 1 articles about Benzenamine, N-[2-(diphenylphosphino)cyclopentylidene]-2,6-bis(1-methylethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: N-(2,6-diisopropylphenyl)cyclopentylideneimine

: 494191-96-7
2,6-diisopropyl-N-(2-diphenylphosphino-cyclopentylidene)aniline

Guidance literature:: N-(2,6-diisopropylphenyl)cyclopentylideneimine; With lithium diisopropyl amide; In diethyl ether; at -78 ℃; Inert atmosphere;

chloro-diphenylphosphine; In diethyl ether; at -78 ℃; Inert atmosphere;
DOI:10.1021/om400688v

Reference yield: 99.0%

: 28923-39-9
nickel(II) bromide dimethoxyethane

: 494191-96-7
2,6-diisopropyl-N-(2-diphenylphosphino-cyclopentylidene)aniline

: 494192-32-4
[(2,6-diisopropyl-N-(2-diphenylphosphino-cyclopentylidene)aniline-κ2-P,N)di(bromo)nickel(II)]

Guidance literature:: In dichloromethane; Sonication; under Ar; 0.4 mmol of Ni-contg. compd. were suspended in CH2Cl2 at room temp. with the aid of an ultrasound bath and slowly reacted with a soln.of 1.00 equiv. of a ligand in the same solvent; stirring for 1 h; the soln. was filtered and the filtrate was concd., washed with n-pentane and dried in vac.; the complex was crystd. from CH2Cl2; elem. anal.;
DOI:10.1016/S0022-328X(02)01903-4

Reference yield: 97.0%

: chloromethyl(1,5-cyclooctadiene)palladium(II)

: 494191-96-7
2,6-diisopropyl-N-(2-diphenylphosphino-cyclopentylidene)aniline

: 494192-08-4
[(2,6-diisopropyl-N-(2-diphenylphosphino-cyclopentylidene)aniline-κ2-P,N)(chloro)(methyl)palladium(II)]

Guidance literature:: In dichloromethane; byproducts: 1,5-cyclooctadiene; under Ar; to a soln. of Pd-contg. compd. (1.990 mmol) in CH2Cl2 kept under stirring, a soln. of a ligand (1.990 mmol) in the same solvent was added dropwise at room temp.; stirring for 30 min; the solvent was reduced in vac.; the complex was pptd. by addn. of n-pentane; the solid was filtered, washed with pentane and dried; elem. anal.;
DOI:10.1016/S0022-328X(02)01903-4