[(2,6-diisopropyl-N-(2-diphenylphosphino-cyclopentylidene)aniline-κ2-P,N)(chloro)(methyl)palladium(II)]

Base Information

Chemical Name:[(2,6-diisopropyl-N-(2-diphenylphosphino-cyclopentylidene)aniline-κ2-P,N)(chloro)(methyl)palladium(II)]
CAS No.:494192-08-4
Molecular Formula:C₃₀H₃₇ClNPPd
Molecular Weight:584.477
Hs Code.:

Synonyms:

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Chemical Property of [(2,6-diisopropyl-N-(2-diphenylphosphino-cyclopentylidene)aniline-κ2-P,N)(chloro)(methyl)palladium(II)]

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Technology Process of [(2,6-diisopropyl-N-(2-diphenylphosphino-cyclopentylidene)aniline-κ2-P,N)(chloro)(methyl)palladium(II)]

There total 1 articles about [(2,6-diisopropyl-N-(2-diphenylphosphino-cyclopentylidene)aniline-κ2-P,N)(chloro)(methyl)palladium(II)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: chloromethyl(1,5-cyclooctadiene)palladium(II)

: 494191-96-7
2,6-diisopropyl-N-(2-diphenylphosphino-cyclopentylidene)aniline

: 494192-08-4
[(2,6-diisopropyl-N-(2-diphenylphosphino-cyclopentylidene)aniline-κ2-P,N)(chloro)(methyl)palladium(II)]

Guidance literature:: In dichloromethane; byproducts: 1,5-cyclooctadiene; under Ar; to a soln. of Pd-contg. compd. (1.990 mmol) in CH2Cl2 kept under stirring, a soln. of a ligand (1.990 mmol) in the same solvent was added dropwise at room temp.; stirring for 30 min; the solvent was reduced in vac.; the complex was pptd. by addn. of n-pentane; the solid was filtered, washed with pentane and dried; elem. anal.;
DOI:10.1016/S0022-328X(02)01903-4

Reference yield: 96.0%

: 26042-64-8
silver hexafluoroantimonate

: 494192-08-4
[(2,6-diisopropyl-N-(2-diphenylphosphino-cyclopentylidene)aniline-κ2-P,N)(chloro)(methyl)palladium(II)]

: 75-05-8,26809-02-9
acetonitrile

: 494192-18-6
[(acetonitrile)(2,6-diisopropyl-N-(2-diphenylphosphino-cyclopentylidene)aniline-κ2-P,N)(methyl)palladium(II)]hexafluoroantimonate

Guidance literature:: In dichloromethane; byproducts: AgCl; under Ar; to a soln. of Pd-contg. compd. (0.795 mmol) in CH2Cl2 contg. MeCN and kept under stirring, AgSbF6 (0.805 mmol) suspended in the same solvent was added at a temp. 0-20°C; stirring for 5 min; AgCl was filtered and the soln. concd.; the complex was pptd. by addn. of n-pentane; the complex was isolated and dried in vac.; elem. anal.;
DOI:10.1016/S0022-328X(02)01903-4