5-[(4-METHOXYPHENYL)ETHYNYL]-1,3-BENZODIOXOLE

Base Information

Chemical Name:5-[(4-METHOXYPHENYL)ETHYNYL]-1,3-BENZODIOXOLE
CAS No.:495413-04-2
Molecular Formula:C16H12O3
Molecular Weight:252.269
Hs Code.:
Mol file:495413-04-2.mol

Synonyms:5-[2-(4-METHOXYPHENYL)ETHYNYL]-1,3-BENZODIOXOLE;(4-methoxyphenyl)-(benzo-1,3-dioxol-5-yl)-ethyne;

Suppliers and Price of 5-[(4-METHOXYPHENYL)ETHYNYL]-1,3-BENZODIOXOLE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
5-[2-(4-METHOXYPHENYL)ETHYNYL]-1,3-BENZODIOXOLE 95.00%
5MG
$ 502.39

Total 0 raw suppliers

Chemical Property of 5-[(4-METHOXYPHENYL)ETHYNYL]-1,3-BENZODIOXOLE

Chemical Property:

PSA：27.69000
LogP:2.82370

Purity/Quality:: 5-[2-(4-METHOXYPHENYL)ETHYNYL]-1,3-BENZODIOXOLE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5-[(4-METHOXYPHENYL)ETHYNYL]-1,3-BENZODIOXOLE

There total 6 articles about 5-[(4-METHOXYPHENYL)ETHYNYL]-1,3-BENZODIOXOLE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 623-12-1
4-chloromethoxybenzene

: 4-(benzo[d][1,3]dioxol-5-yl)-2-methylbut-3-yn-2-ol

: 495413-04-2
5-((4-methoxyphenyl)ethynyl)benzo[d][1,3]dioxole

Guidance literature:: With {(Pd{Fe(η5-C5H5)(η5-C5H3C(CH3)=NC6H4CH3-4)}(μ-Cl))2}; potassium carbonate; XPhos; In acetonitrile; at 110 ℃; for 16h; Inert atmosphere;
DOI:10.1021/jo4014657

Reference yield: 66.0%

: 10231-46-6
3-(benzo[d][1,3]dioxol-5-yl)propiolic acid

: 21130-91-6
triethoxy(4-methoxyphenyl)silane

: 495413-04-2
5-((4-methoxyphenyl)ethynyl)benzo[d][1,3]dioxole

Guidance literature:: With silver(II) fluoride; bis-diphenylphosphinomethane; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In toluene; at 60 ℃; for 6h;
DOI:10.1016/j.tetlet.2016.08.095

Reference yield: 46.0%

: 33675-41-1
1-bromo-2-(4-methoxyphenyl)acetylene

: 17680-04-5
(3,4-methylenedioxy)phenylmagnesium bromide

: 495413-04-2
5-((4-methoxyphenyl)ethynyl)benzo[d][1,3]dioxole

Guidance literature:: (3,4-methylenedioxy)phenylmagnesium bromide; With copper(l) chloride; In tetrahydrofuran; at 25 ℃; for 0.333333h;

1-bromo-2-(4-methoxyphenyl)acetylene; With iron(III)-acetylacetonate; at 20 ℃;
DOI:10.1002/ejoc.201000924