3,13-Dioxa-4,12-disila-6,10-distannapentadecane, 2,4,4,12,12,14-hexamethyl-6,6,10,10-tetraphenyl-

Base Information

Chemical Name:3,13-Dioxa-4,12-disila-6,10-distannapentadecane, 2,4,4,12,12,14-hexamethyl-6,6,10,10-tetraphenyl-
CAS No.:496854-20-7
Molecular Formula:C39H56O2Si2Sn2
Molecular Weight:850.463
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,13-Dioxa-4,12-disila-6,10-distannapentadecane, 2,4,4,12,12,14-hexamethyl-6,6,10,10-tetraphenyl-

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Technology Process of 3,13-Dioxa-4,12-disila-6,10-distannapentadecane, 2,4,4,12,12,14-hexamethyl-6,6,10,10-tetraphenyl-

There total 1 articles about 3,13-Dioxa-4,12-disila-6,10-distannapentadecane, 2,4,4,12,12,14-hexamethyl-6,6,10,10-tetraphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 223668-34-6
1,3-bis(diphenylfluorostannyl)propane

: 122588-50-5
(dimethylisopropoxysilyl)methylmagnesium chloride

: 496854-20-7
1,3-([(dimethylisopropoxysilyl)methyl]diphenylstannyl)propane

Guidance literature:: In tetrahydrofuran; under Ar to suspn. 1,3-bis(diphenylfluorostannyl)propane in THF was added dropwise at 0°C soln. Me2(i-PrO)SiCH2MgCl in THF and stirred atroom temp. for 15 h; solvent was removed in vacuo, hexane was added, soln. was filtered, solvent was removed in vacuo;
DOI:10.1021/om020740b

Reference yield: 41.0%

: 496854-20-7
1,3-([(dimethylisopropoxysilyl)methyl]diphenylstannyl)propane

: mercury dichloride

: 496854-18-3
1,1,5,5-tetrachloro-7,7,9,9-tetramethyl-7,9-disila-1,5-distanna-8-oxacyclodecane

: 100-56-1
phenylmercury(II) chloride

Guidance literature:: In acetone; under Ar HgCl2 in acetone was added dropwise at 0°C over 1 h to soln. 1,3-bis(((dimethylisopropoxysilyl)methyl)diphenylstannyl)propane and stirred for 14 h at room temp.; soln. was filtered, solvent was removedin vacuo, residue was extd. with hot n-hexane, extract was kept overnight at -25°C, ppt. was filtered and dried;
DOI:10.1021/om020740b