Germane, [bis[2,4,6-tris(1-methylethyl)phenyl]stannylene]bis[2,4,6-tris(1-methyleth yl)phenyl]-

Base Information

Chemical Name:Germane, [bis[2,4,6-tris(1-methylethyl)phenyl]stannylene]bis[2,4,6-tris(1-methyleth yl)phenyl]-
CAS No.:496863-87-7
Molecular Formula:C₆₀H₉₂GeSn
Molecular Weight:1004.69
Hs Code.:

Synonyms:

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Chemical Property of Germane, [bis[2,4,6-tris(1-methylethyl)phenyl]stannylene]bis[2,4,6-tris(1-methyleth yl)phenyl]-

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MSDS Files:: SDS file from LookChem

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Technology Process of Germane, [bis[2,4,6-tris(1-methylethyl)phenyl]stannylene]bis[2,4,6-tris(1-methyleth yl)phenyl]-

There total 1 articles about Germane, [bis[2,4,6-tris(1-methylethyl)phenyl]stannylene]bis[2,4,6-tris(1-methyleth yl)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: germanium(II) chloride dioxane

: 108894-99-1
(2,4,6-triisopropylphenyl)magnesium bromide

: tin(ll) chloride

: 496863-87-7
(((CH₃)2CH)3C₆H₂)4GeSn

Guidance literature:: In tetrahydrofuran; 1,4-dioxane; to suspn. GeCl2*dioxane and SnCl2 in THF and dioxane was added at -78°C dropwise soln. Grignard reagent, react. mixt. was allowed to cometo -10°C and stirred at this temp. for 30 min; solvents were distilled off, residue was redissolved in cooled n-pentane, ppt. was filtered off, filtrate was concd. and cooled to -20°C;
DOI:10.1021/om020855f