2-Chloro-5-methylphenanthridin-6(5h)-one

Base Information

Chemical Name:2-Chloro-5-methylphenanthridin-6(5h)-one
CAS No.:54960-76-8
Molecular Formula:C14H10ClNO
Molecular Weight:243.6883
Hs Code.:
NSC Number:141585
DSSTox Substance ID:DTXSID30301173
Nikkaji Number:J3.069.413I
Wikidata:Q82044815

Synonyms:54960-76-8;2-chloro-5-methylphenanthridin-6(5h)-one;NSC141585;DTXSID30301173;NSC-141585

Suppliers and Price of 2-Chloro-5-methylphenanthridin-6(5h)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 2-Chloro-5-methylphenanthridin-6(5h)-one

Chemical Property:

Vapor Pressure:5.88E-08mmHg at 25°C
Boiling Point:440.5°C at 760 mmHg
Flash Point:220.2°C
Density:1.313g/cm³
XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:243.0450916
Heavy Atom Count:17
Complexity:319

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1C2=C(C=C(C=C2)Cl)C3=CC=CC=C3C1=O

Technology Process of 2-Chloro-5-methylphenanthridin-6(5h)-one

There total 18 articles about 2-Chloro-5-methylphenanthridin-6(5h)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1372788-34-5
N-(4-chlorophenyl)-2-iodo-N-methylbenzamide

: 54960-76-8
2-chloro-5-methylphenanthridin-6(5H)-one

Guidance literature:: With di‐μ‐chlorobis [5‐hydroxy‐2‐[1‐(hydroxyimino‐κN) ethyl] phenyl‐κC] palladium (II); potassium carbonate; In N,N-dimethyl acetamide; at 140 ℃; for 24h; Inert atmosphere;
DOI:10.1002/ejoc.201101400

Reference yield: 89.0%

: 1372788-39-0
C₁₄H₁₁BrClNO

: 54960-76-8
2-chloro-5-methylphenanthridin-6(5H)-one

Guidance literature:: With di‐μ‐chlorobis [5‐hydroxy‐2‐[1‐(hydroxyimino‐κN) ethyl] phenyl‐κC] palladium (II); potassium carbonate; In N,N-dimethyl acetamide; at 140 ℃; for 72h; Inert atmosphere;
DOI:10.1002/ejoc.201101400

Reference yield: 83.0%

: 872492-58-5
(4-chloro-2-iodophenyl)methylamine

: 201230-82-2
carbon monoxide

: 88284-48-4
2-(trimethylsilyl)phenyl trifluoromethanesulfonate

: 54960-76-8
2-chloro-5-methylphenanthridin-6(5H)-one

Guidance literature:: With palladium diacetate; tetra-(n-butyl)ammonium iodide; potassium carbonate; cesium fluoride; In water; acetonitrile; at 100 ℃; for 12h; Inert atmosphere; Schlenk technique;
DOI:10.1002/anie.201508340