2-Methylcyclohex-3-en-1-one

Base Information

Chemical Name:2-Methylcyclohex-3-en-1-one
CAS No.:4982-22-3
Molecular Formula:C7H10O
Molecular Weight:110.156
Hs Code.:
DSSTox Substance ID:DTXSID20576055

Synonyms:2-Methylcyclohex-3-en-1-one;4982-22-3;methylcyclohex-3-enone;SCHEMBL768641;DTXSID20576055

Suppliers and Price of 2-Methylcyclohex-3-en-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Methylcyclohex-3-en-1-one

Chemical Property:

XLogP3:1.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:110.073164938
Heavy Atom Count:8
Complexity:124

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1C=CCCC1=O

Technology Process of 2-Methylcyclohex-3-en-1-one

There total 4 articles about 2-Methylcyclohex-3-en-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 70291-22-4
4-hydroxy-4-(hydroxymethyl)-3-methylcyclohexene

: 4982-22-3
2-methylcyclohex-3-en-1-one

Guidance literature:: With sodium periodate; In methanol; water; for 1h; Ambient temperature;
DOI:10.1021/jo00174a008

Reference yield: 20.0%

: 4096-34-8
cyclohex-3-enone

: 74-88-4
methyl iodide

: 4982-22-3
2-methylcyclohex-3-en-1-one

Guidance literature:: cyclohex-3-enone; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 1h;

methyl iodide; In tetrahydrofuran; at -78 ℃; for 12h;
DOI:10.1002/anie.202006841

Reference yield:

: 70291-20-2
4-acetoxy-4-carbomethoxy-3-methylcyclohexene

: 4982-22-3
2-methylcyclohex-3-en-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / lithium tetrahydroaluminate / diethyl ether / 1 h / 0 °C

2: 74 percent / sodium metaperiodate / methanol; H₂O / 1 h / Ambient temperature

With sodium periodate; lithium aluminium tetrahydride; In methanol; diethyl ether; water;
DOI:10.1021/jo00174a008