3,4-dihydroxy-12,13-epoxytrichothec-9-en-15-oic acid

Base Information

Chemical Name:3,4-dihydroxy-12,13-epoxytrichothec-9-en-15-oic acid
CAS No.:81331-37-5
Molecular Formula:C₁₅H₂₀O₆
Molecular Weight:296.32
Hs Code.:

Synonyms:

Suppliers and Price of 3,4-dihydroxy-12,13-epoxytrichothec-9-en-15-oic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 6 raw suppliers

Chemical Property of 3,4-dihydroxy-12,13-epoxytrichothec-9-en-15-oic acid

Chemical Property:

Vapor Pressure:5.27E-13mmHg at 25°C
Boiling Point:520.4°C at 760 mmHg
Flash Point:197.3°C
Density:1.48g/cm³

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 3,4-dihydroxy-12,13-epoxytrichothec-9-en-15-oic acid

There total 5 articles about 3,4-dihydroxy-12,13-epoxytrichothec-9-en-15-oic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₀H₂₈O₇

: 81331-37-5
3α,4β-dihydroxyscirpene-15-carboxylic acid

Guidance literature:: With hydrogenchloride; In ethanol; for 18h; Yield given; Ambient temperature;
DOI:10.1021/jm00347a018

Reference yield:

: 2270-40-8,106454-36-8,28776-47-8
anguidine

: 81331-37-5
3α,4β-dihydroxyscirpene-15-carboxylic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 72 percent / p-toluenesulfonic acid / CH₂Cl₂ / 2 h / Ambient temperature

2: 17 percent / aq. NH₄OH / methanol; tetrahydrofuran / 168 h / Ambient temperature

3: 72 percent / pyridinium chlorochromate, sodium acetate / CH₂Cl₂ / 1 h / Ambient temperature

4: 0.1 M aq. KMnO₄ / acetone / 1 h / Ambient temperature

5: 1 N aq. HCl / ethanol / 18 h / Ambient temperature

With hydrogenchloride; ammonium hydroxide; potassium permanganate; sodium acetate; toluene-4-sulfonic acid; pyridinium chlorochromate; In tetrahydrofuran; methanol; ethanol; dichloromethane; acetone;
DOI:10.1021/jm00347a018

Reference yield:

: 81331-31-9
4β-hydroxy-3α-O-(2-tetrahydropyranyl)scirpene-15-carboxaldehyde

: 81331-37-5
3α,4β-dihydroxyscirpene-15-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 0.1 M aq. KMnO₄ / acetone / 1 h / Ambient temperature

2: 1 N aq. HCl / ethanol / 18 h / Ambient temperature

With hydrogenchloride; potassium permanganate; In ethanol; acetone;
DOI:10.1021/jm00347a018