hexahydro-2a,4a,6a-triaza-6b-phosphacyclopenta[cd]pentalene 6b-oxide

Base Information

Chemical Name:hexahydro-2a,4a,6a-triaza-6b-phosphacyclopenta[cd]pentalene 6b-oxide
CAS No.:71771-37-4
Molecular Formula:C₆H₁₂N₃OP
Molecular Weight:173.155
Hs Code.:

Synonyms:

Suppliers and Price of hexahydro-2a,4a,6a-triaza-6b-phosphacyclopenta[cd]pentalene 6b-oxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 7 raw suppliers

Chemical Property of hexahydro-2a,4a,6a-triaza-6b-phosphacyclopenta[cd]pentalene 6b-oxide

Chemical Property:

Vapor Pressure:0.00123mmHg at 25°C
Boiling Point:299°Cat760mmHg
Flash Point:134.6°C
Density:1.47g/cm³

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of hexahydro-2a,4a,6a-triaza-6b-phosphacyclopenta[cd]pentalene 6b-oxide

There total 2 articles about hexahydro-2a,4a,6a-triaza-6b-phosphacyclopenta[cd]pentalene 6b-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: 4730-54-5
1,4,7-triazacyclononane

: 71771-37-4
hexahydro-2a,4a,6a-triaza-6b-phospha-cyclopenta[cd]pentalene 6b-oxide

Guidance literature:: With triethylamine; trichlorophosphate; In benzene; for 2h; Ambient temperature;
DOI:10.1039/a704966h

Reference yield:

: 52667-89-7
N,N',N-tris(p-toluenesulfonyl)-1,4,7-triazacyclononane

: 71771-37-4
hexahydro-2a,4a,6a-triaza-6b-phospha-cyclopenta[cd]pentalene 6b-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / conc. H₂SO₄ / 120 h / 120 °C

2: 16 percent / POCl₃, Et₃N / benzene / 2 h / Ambient temperature

With sulfuric acid; triethylamine; trichlorophosphate; In benzene;
DOI:10.1039/a704966h