Technology Process of Benzenemethanamine, N-[[(2E)-4-phenyl-2-pentenyl]oxy]-
There total 5 articles about Benzenemethanamine, N-[[(2E)-4-phenyl-2-pentenyl]oxy]- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
benzaldehyde (E)-O-(4-phenylpent-2-enyl)oxime;
With
pyridine; borane pyridine;
In
ethanol;
at 20 ℃;
With
hydrogenchloride;
In
ethanol;
at 20 ℃;
for 2h;
Further stages.;
DOI:10.1039/b207069n
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 100 percent / tetrahydrofuran / 73 h / -78 - 20 °C
2.1: 75 percent / DIBAL-H / CH2Cl2 / -78 - 20 °C
3.1: PBr3 / diethyl ether / 18 h / 20 °C
4.1: t-BuOK / tetrahydrofuran / 0.5 h
4.2: 1.05 g / tetrahydrofuran; diethyl ether / 72 h / 20 °C
5.1: BH3*pyridine; pyridine / ethanol / 20 °C
5.2: 78 percent / HCl / ethanol / 2 h / 20 °C
With
pyridine; borane pyridine; potassium tert-butylate; phosphorus tribromide; diisobutylaluminium hydride;
In
tetrahydrofuran; diethyl ether; ethanol; dichloromethane;
1.1: Wittig reaction;
DOI:10.1039/b207069n
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 75 percent / DIBAL-H / CH2Cl2 / -78 - 20 °C
2.1: PBr3 / diethyl ether / 18 h / 20 °C
3.1: t-BuOK / tetrahydrofuran / 0.5 h
3.2: 1.05 g / tetrahydrofuran; diethyl ether / 72 h / 20 °C
4.1: BH3*pyridine; pyridine / ethanol / 20 °C
4.2: 78 percent / HCl / ethanol / 2 h / 20 °C
With
pyridine; borane pyridine; potassium tert-butylate; phosphorus tribromide; diisobutylaluminium hydride;
In
tetrahydrofuran; diethyl ether; ethanol; dichloromethane;
DOI:10.1039/b207069n
