3-Chloro-n-(2-chloroethyl)benzamide

Base Information

Chemical Name:3-Chloro-n-(2-chloroethyl)benzamide
CAS No.:15258-03-4
Molecular Formula:C₉H₉Cl₂NO
Molecular Weight:218.083
Hs Code.:
NSC Number:101533
DSSTox Substance ID:DTXSID50295368
Wikidata:Q82035264

Synonyms:3-chloro-n-(2-chloroethyl)benzamide;15258-03-4;NSC101533;NCIOpen2_006825;DTXSID50295368;AKOS010542270;NSC-101533

Suppliers and Price of 3-Chloro-n-(2-chloroethyl)benzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 3-Chloro-n-(2-chloroethyl)benzamide

Chemical Property:

Vapor Pressure:2.99E-05mmHg at 25°C
Boiling Point:356.1°Cat760mmHg
Flash Point:169.2°C
Density:1.285g/cm³
XLogP3:2.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:217.0061193
Heavy Atom Count:13
Complexity:175

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC(=C1)Cl)C(=O)NCCCl

Technology Process of 3-Chloro-n-(2-chloroethyl)benzamide

There total 3 articles about 3-Chloro-n-(2-chloroethyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 57728-64-0
3-Chloro-N-(2-hydroxy-ethyl)-benzamide

: 15258-03-4
3-Chloro-N-(2-chloro-ethyl)-benzamide

Guidance literature:: With thionyl chloride; In chloroform; for 0.5h; Heating;
DOI:10.1021/jo00143a029

Reference yield:

: 618-46-2
m-Chlorobenzoyl chloride

: 15258-03-4
3-Chloro-N-(2-chloro-ethyl)-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / 1.) 5 deg C, 2.) RT, 0.5 h

2: thionyl chloride / CHCl₃ / 0.5 h / Heating

With thionyl chloride; In dichloromethane; chloroform;
DOI:10.1021/jo00143a029