2-Butyramido-3-Nitrophenyl Trifluoromethanesulfonate

Base Information

Chemical Name:2-Butyramido-3-Nitrophenyl Trifluoromethanesulfonate
CAS No.:500991-98-0
Molecular Formula:C11H11F3N2O6S
Molecular Weight:356.279
Hs Code.:
Mol file:500991-98-0.mol

Synonyms:

Suppliers and Price of 2-Butyramido-3-Nitrophenyl Trifluoromethanesulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
2-Butyramido-3-nitrophenyltrifluoromethanesulfonate 95+%
5g
$ 1116.00

Crysdot
2-Butyramido-3-nitrophenyltrifluoromethanesulfonate 95+%
1g
$ 371.00

Total 3 raw suppliers

Chemical Property of 2-Butyramido-3-Nitrophenyl Trifluoromethanesulfonate

Chemical Property:

Melting Point:119-119.5 °C(Solv: dichloromethane (75-09-2); hexane (110-54-3))
Boiling Point:471.9±45.0 °C(Predicted)
PKA:12.51±0.70(Predicted)
PSA：126.67000
Density:1.557±0.06 g/cm3(Predicted)
LogP:4.23880

Purity/Quality:

97% ^*data from raw suppliers

2-Butyramido-3-nitrophenyltrifluoromethanesulfonate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Butyramido-3-Nitrophenyl Trifluoromethanesulfonate

There total 2 articles about 2-Butyramido-3-Nitrophenyl Trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 500991-93-5
N-(2'-hydroxy-6'-nitrophenyl)butyramide

: 500991-98-0
N-[6'-nitro-2'-(((trifluoromethane)sulfonyl)oxy)phenyl]butyramide

Guidance literature:: With triethylamine; In acetonitrile; at -5 - 0 ℃; for 6h;
DOI:10.1016/S0040-4039(02)01851-8

Reference yield:

: 603-85-0
2-Amino-3-nitrophenol

: 500991-98-0
N-[6'-nitro-2'-(((trifluoromethane)sulfonyl)oxy)phenyl]butyramide

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / NaH / tetrahydrofuran / 24 h / 20 °C

2: 94 percent / triethylamine / CH₂Cl₂ / 7 h / cooling

With sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tet.2004.09.034

Reference yield: 98.0%

: 14235-81-5
4-Ethynylaniline

: 500991-98-0
N-[6'-nitro-2'-(((trifluoromethane)sulfonyl)oxy)phenyl]butyramide

: 1253396-05-2
N-{[6-nitro-2-(4-aminophenyl)ethynyl]phenyl}butyramide

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetra-(n-butyl)ammonium iodide; triethylamine; In acetonitrile; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/cmdc.201000228