9H-Bis(1,2,4)triazolo(4,3-a:3',4'-d)(1,5)benzodiazepine, 6,12-diphenyl-9-methyl-

Base Information

Chemical Name:9H-Bis(1,2,4)triazolo(4,3-a:3',4'-d)(1,5)benzodiazepine, 6,12-diphenyl-9-methyl-
CAS No.:133118-27-1
Molecular Formula:C₂₄H₁₈N₆
Molecular Weight:390.447
Hs Code.:
DSSTox Substance ID:DTXSID20157969
Wikidata:Q83026126

Synonyms:BRN 4212663;9H-Bis(1,2,4)triazolo(4,3-a:3',4'-d)(1,5)benzodiazepine, 6,12-diphenyl-9-methyl-;133118-27-1;6,12-Diphenyl-9-methyl-9H-bis(1,2,4)triazolo(4,3-a:3',4'-d)(1,5)benzodiazepine;DTXSID20157969;C24H18N6;C24-H18-N6;LS-44751;9H-Bis[1,2,4]triazolo[3,4-d:4',3'-a][1,5]benzodiazepine, 6,12-diphenyl-9-methyl-

Suppliers and Price of 9H-Bis(1,2,4)triazolo(4,3-a:3',4'-d)(1,5)benzodiazepine, 6,12-diphenyl-9-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 2 raw suppliers

Chemical Property of 9H-Bis(1,2,4)triazolo(4,3-a:3',4'-d)(1,5)benzodiazepine, 6,12-diphenyl-9-methyl-

Chemical Property:

Boiling Point:683.2°Cat760mmHg
Flash Point:367°C
Density:1.35g/cm³
XLogP3:4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:390.15929460
Heavy Atom Count:30
Complexity:538

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1C2=NN=C(N2C3=CC=CC=C3N4C1=NN=C4C5=CC=CC=C5)C6=CC=CC=C6

Technology Process of 9H-Bis(1,2,4)triazolo(4,3-a:3',4'-d)(1,5)benzodiazepine, 6,12-diphenyl-9-methyl-

There total 4 articles about 9H-Bis(1,2,4)triazolo(4,3-a:3',4'-d)(1,5)benzodiazepine, 6,12-diphenyl-9-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

: 133118-31-7
3-methyl-N,N-dimethyl-4-(methylthio)-3H-1,5-benzodiazepin-2-amine

: 613-94-5
benzoic acid hydrazide

: 133118-18-0
4-methyl-N,N-dimethyl-1-phenyl-4H-<1,2,4>triazolo<4,3-a><1,5>benzodiazepin-5-amine

: 133118-27-1
9-methyl-6,12-diphenyl-9H-bis<1,2,4>triazolo<4,3-a:3',4'-d><1,5>benzodiazepine

Guidance literature:: In various solvent(s); at 200 ℃; for 1h;
DOI:10.1016/0223-5234(90)90133-N

Reference yield:

: 133118-33-9
4-(dimethylamino)-1,3-dihydro-3-methyl-2H-1,5-benzodiazepin-2-one

: 133118-27-1
9-methyl-6,12-diphenyl-9H-bis<1,2,4>triazolo<4,3-a:3',4'-d><1,5>benzodiazepine

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / Lawesson's reagent / toluene / 0.5 h / 100 °C

2: 1.) NaH / 1.) THF, toluene, 50 deg C, 45 min, 2.) 50 deg C, 90 min

3: 13 percent / various solvent(s) / 1 h / 200 °C

With Lawessons reagent; sodium hydride; In toluene;
DOI:10.1016/0223-5234(90)90133-N

Reference yield:

: 133118-34-0
4-(dimethylamino)-1,3-dihydro-3-methyl-2H-1,5-benzodiazepin-2-thione

: 133118-27-1
9-methyl-6,12-diphenyl-9H-bis<1,2,4>triazolo<4,3-a:3',4'-d><1,5>benzodiazepine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) THF, toluene, 50 deg C, 45 min, 2.) 50 deg C, 90 min

2: 13 percent / various solvent(s) / 1 h / 200 °C

With sodium hydride; In various solvent(s);
DOI:10.1016/0223-5234(90)90133-N