1,2-Ethanediamine, N,N'-dinitroso-N,N'-bis(phenylmethyl)-

Base Information

• Chemical Name: 1,2-Ethanediamine, N,N'-dinitroso-N,N'-bis(phenylmethyl)-
• CAS No.: 69239-61-8
• Molecular Formula: C16H18N4O2
• Molecular Weight: 298.3397
• DSSTox Substance ID: DTXSID90219301
• Nikkaji Number: J1.005.440K
• Wikidata: Q83096222

Synonyms:1,2-Ethanediamine, N,N'-dinitroso-N,N'-bis(phenylmethyl)-;69239-61-8;N,N'-Dinitroso-N,N'-bis(phenylmethyl)-1,2-ethanediamine;DTXSID90219301

Chemical Property of 1,2-Ethanediamine, N,N'-dinitroso-N,N'-bis(phenylmethyl)-

Chemical Property:

• Boiling Point: 560.2°Cat760mmHg
• Flash Point: 292.6°C
• Density: 1.15g/cm³
• XLogP3: 3.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 7
• Exact Mass: 298.14297583
• Heavy Atom Count: 22
• Complexity: 296

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)CN(CCN(CC2=CC=CC=C2)N=O)N=O

Technology Process of 1,2-Ethanediamine, N,N'-dinitroso-N,N'-bis(phenylmethyl)-

There total 3 articles about 1,2-Ethanediamine, N,N'-dinitroso-N,N'-bis(phenylmethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

N,N'-Dibenzylethylenediamine (140-28-3,87170-83-0) → N,N'-Dibenzyl-N,N'-dinitroso-1,2-diaminoethane (69239-61-8)

Guidance literature:

With hydrogenchloride; sodium nitrite; for 20h; Heating;

DOI:10.1039/b101030l

Reference yield:

N,N'-bis(benzyliden)ethylendiamine (104-71-2) → N,N'-Dibenzyl-N,N'-dinitroso-1,2-diaminoethane (69239-61-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / sodium borohydride / ethanol

2: 94 percent / sodium nitrite, HCl / H₂O

With hydrogenchloride; sodium tetrahydroborate; sodium nitrite; In ethanol; water;

DOI:10.1016/S0040-4039(98)01968-6

Reference yield:

N,N'-dibenzylethylenediamine dihydrochloride (3412-76-8,63674-12-4) → N,N'-Dibenzyl-N,N'-dinitroso-1,2-diaminoethane (69239-61-8)

Guidance literature:

With water; sodium nitrite;

upstream raw materials:

N,N'-dibenzylethylenediamine dihydrochloride

N,N'-Dibenzylethylenediamine

N,N'-bis(benzyliden)ethylendiamine

Downstream raw materials:

[Benzyl-(2-{[1-methoxycarbonyl-1-phenyl-meth-(E)-ylidene]-hydrazino}-ethyl)-hydrazono]-phenyl-acetic acid methyl ester

2-[Benzyl-(2-{[1-dimethylcarbamoyl-1-phenyl-meth-(E)-ylidene]-hydrazino}-ethyl)-hydrazono]-N,N-dimethyl-2-phenyl-acetamide

copper (II) dichloro(N,N'-dibenzylethylenediamine)

N,N'-Diamino-N,N'-dibenzyl-1,2-diaminoethane

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