2,3-Difluoro-1,4-diiodobenzene

Base Information

Chemical Name:2,3-Difluoro-1,4-diiodobenzene
CAS No.:501433-06-3
Molecular Formula:C6H2F2I2
Molecular Weight:365.888
Hs Code.:2903999090
European Community (EC) Number:816-297-2
DSSTox Substance ID:DTXSID00471953
Nikkaji Number:J1.831.281F
Wikidata:Q82300661
Mol file:501433-06-3.mol

Synonyms:2,3-Difluoro-1,4-diiodobenzene;501433-06-3;MFCD22273735;Benzene, 2,3-difluoro-1,4-diiodo-;SCHEMBL1425995;DTXSID00471953;AMY28443;BVA43306;AKOS024263909;PS-10234;SY075887;CS-0060323;AS-813/43501995

Suppliers and Price of 2,3-Difluoro-1,4-diiodobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2,3-Difluoro-1,4-diiodobenzene
500mg
$ 130.00

SynQuest Laboratories
2,3-Difluoro-1,4-diiodobenzene
1 g
$ 101.00

SynQuest Laboratories
2,3-Difluoro-1,4-diiodobenzene
5 g
$ 333.00

Oakwood
2,3-Difluoro-1,4-diiodobenzene 98%
5g
$ 270.00

Apolloscientific
2,3-Difluoro-1,4-diiodobenzene
5g
$ 295.00

Apolloscientific
2,3-Difluoro-1,4-diiodobenzene
1g
$ 89.00

Ambeed
2,3-Difluoro-1,4-diiodobenzene 95%
1g
$ 77.00

Ambeed
2,3-Difluoro-1,4-diiodobenzene 95%
5g
$ 278.00

Ambeed
2,3-Difluoro-1,4-diiodobenzene 95%
10g
$ 482.00

Alichem
2,3-Difluoro-1,4-diiodobenzene
25g
$ 1156.48

Total 17 raw suppliers

Chemical Property of 2,3-Difluoro-1,4-diiodobenzene

Chemical Property:

Boiling Point:271.3±35.0 °C(Predicted)
PSA：0.00000
Density:2.576±0.06 g/cm3(Predicted)
LogP:3.17400
Storage Temp.:2-8°C(protect from light)
XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:365.82140
Heavy Atom Count:10
Complexity:106

Purity/Quality:

95% ^*data from raw suppliers

2,3-Difluoro-1,4-diiodobenzene ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C(=C1I)F)F)I

Technology Process of 2,3-Difluoro-1,4-diiodobenzene

There total 2 articles about 2,3-Difluoro-1,4-diiodobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 64248-57-3
1-iodo-2,3-difluorobenzene

: 501433-06-3
2,3-difluoro-1,4-diiodobenzene

Guidance literature:: With iodine; lithium diisopropyl amide; In tetrahydrofuran; hexane; at -75 ℃;
DOI:10.1002/1099-0690(200210)2002:19<3351::AID-EJOC3351>3.0.CO;2-I

Reference yield: 76.0%

: 367-11-3
ortho-difluorobenzene

: 501433-06-3
2,3-difluoro-1,4-diiodobenzene

Guidance literature:: ortho-difluorobenzene; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

With iodine; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 4h; Inert atmosphere;
DOI:10.3762/bjoc.15.132

Reference yield: 92.0%

: 1066-54-2
trimethylsilylacetylene

: 501433-06-3
2,3-difluoro-1,4-diiodobenzene

: 1,4-bis(2-trimethylsilylethynyl)-2,3-difluorobenzene

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In tetrahydrofuran; at 70 ℃; for 16h; Inert atmosphere;
DOI:10.3762/bjoc.15.132