Acetamide, N-(2-(4-bromobenzoyl)-8,9-dihydro-8,8-dimethyl-5-phenyl-6H-furo(2,3-b)pyrano(4,3-d)pyridin-1-yl)-

Base Information

Chemical Name:Acetamide, N-(2-(4-bromobenzoyl)-8,9-dihydro-8,8-dimethyl-5-phenyl-6H-furo(2,3-b)pyrano(4,3-d)pyridin-1-yl)-
CAS No.:172985-40-9
Molecular Formula:C₂₇H₂₃BrN₂O₄
Molecular Weight:519.395
Hs Code.:
DSSTox Substance ID:DTXSID20169481
Wikidata:Q83039192
Mol file:172985-40-9.mol

Synonyms:C27H23BrN2O4;172985-40-9;Acetamide, N-(2-(4-bromobenzoyl)-8,9-dihydro-8,8-dimethyl-5-phenyl-6H-furo(2,3-b)pyrano(4,3-d)pyridin-1-yl)-;Oprea1_709124;DTXSID20169481;C27-H23-Br-N2-O4;STL580981;AKOS030506241;LS-8308;N-{2-[(4-bromophenyl)carbonyl]-8,8-dimethyl-5-phenyl-8,9-dihydro-6H-furo[2,3-b]pyrano[4,3-d]pyridin-1-yl}acetamide

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Acetamide, N-(2-(4-bromobenzoyl)-8,9-dihydro-8,8-dimethyl-5-phenyl-6H-furo(2,3-b)pyrano(4,3-d)pyridin-1-yl)-

Chemical Property:

Vapor Pressure:4.22E-22mmHg at 25°C
Boiling Point:745.5°Cat760mmHg
Flash Point:404.7°C
Density:1.409g/cm³
XLogP3:5.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:518.08412
Heavy Atom Count:34
Complexity:762

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)NC1=C(OC2=C1C3=C(COC(C3)(C)C)C(=N2)C4=CC=CC=C4)C(=O)C5=CC=C(C=C5)Br

Technology Process of Acetamide, N-(2-(4-bromobenzoyl)-8,9-dihydro-8,8-dimethyl-5-phenyl-6H-furo(2,3-b)pyrano(4,3-d)pyridin-1-yl)-

There total 2 articles about Acetamide, N-(2-(4-bromobenzoyl)-8,9-dihydro-8,8-dimethyl-5-phenyl-6H-furo(2,3-b)pyrano(4,3-d)pyridin-1-yl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.1%

: 75-36-5
acetyl chloride

: 172985-31-8
(1-Amino-8,8-dimethyl-5-phenyl-8,9-dihydro-6H-3,7-dioxa-4-aza-cyclopenta[a]naphthalen-2-yl)-(4-bromo-phenyl)-methanone

: 172985-40-9
N-[2-(4-Bromo-benzoyl)-8,8-dimethyl-5-phenyl-8,9-dihydro-6H-3,7-dioxa-4-aza-cyclopenta[a]naphthalen-1-yl]-acetamide

Guidance literature:: In 1,4-dioxane; Heating;
DOI:10.1007/BF02219066

Reference yield:

: 6-[2-(4-Bromo-phenyl)-2-oxo-ethoxy]-3,3-dimethyl-8-phenyl-3,4-dihydro-1H-pyrano[3,4-c]pyridine-5-carbonitrile

: 172985-40-9
N-[2-(4-Bromo-benzoyl)-8,8-dimethyl-5-phenyl-8,9-dihydro-6H-3,7-dioxa-4-aza-cyclopenta[a]naphthalen-1-yl]-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 83.3 percent / NaOEt / ethanol / Heating

2: 74.1 percent / dioxane / Heating

With sodium ethanolate; In 1,4-dioxane; ethanol;
DOI:10.1007/BF02219066