N,N-bis(2-chloroethyl)-4-nitrobenzenesulfonamide

Base Information

Chemical Name:N,N-bis(2-chloroethyl)-4-nitrobenzenesulfonamide
CAS No.:90876-33-8
Molecular Formula:C10H12 Cl2 N2 O4 S
Molecular Weight:327.188
Hs Code.:
NSC Number:57823
DSSTox Substance ID:DTXSID60288842
Wikidata:Q82025953
Mol file:90876-33-8.mol

Synonyms:90876-33-8;N,N-bis(2-chloroethyl)-4-nitrobenzenesulfonamide;NSC57823;DTXSID60288842;N,N-BIS(2-CHLOROETHYL)-4-NITRO-BENZENESULFONAMIDE;NSC-57823;AKOS020918120

Suppliers and Price of N,N-bis(2-chloroethyl)-4-nitrobenzenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of N,N-bis(2-chloroethyl)-4-nitrobenzenesulfonamide

Chemical Property:

Vapor Pressure:3.96E-09mmHg at 25°C
Boiling Point:473.4°Cat760mmHg
Flash Point:240.1°C
PSA：91.58000
Density:1.469g/cm³
LogP:3.66710
XLogP3:2.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:6
Exact Mass:325.9894834
Heavy Atom Count:19
Complexity:379

Purity/Quality:: 99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1[N+](=O)[O-])S(=O)(=O)N(CCCl)CCCl

Technology Process of N,N-bis(2-chloroethyl)-4-nitrobenzenesulfonamide

There total 4 articles about N,N-bis(2-chloroethyl)-4-nitrobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 18226-07-8
4-nitro-N,N-bis(2-hydroxyethyl)benzenesulfonamide

: 90876-33-8
N,N-bis(2-chloroethyl)-p-nitrobenzenesulfonamide

Guidance literature:: With thionyl chloride; at 110 ℃; for 1h;

Reference yield:

: 334-22-5
N,N-bis(chloro-2-ethyl)amine

: 98-74-8
4-Nitrobenzenesulfonyl chloride

: 90876-33-8
N,N-bis(2-chloroethyl)-p-nitrobenzenesulfonamide

Guidance literature:: DOI:10.1039/jr9590003616

Reference yield:

: 98-74-8
4-Nitrobenzenesulfonyl chloride

: 90876-33-8
N,N-bis(2-chloroethyl)-p-nitrobenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / water; dichloromethane / 1 h

1.2: 6 h / 25 - 30 °C

2.1: thionyl chloride / 1 h / 110 °C

With thionyl chloride; sodium hydroxide; In dichloromethane; water;