2-(Naphthalen-1-yl)-2,3-dihydro-1h-1,3,2-benzodiazaborole

Base Information

Chemical Name:2-(Naphthalen-1-yl)-2,3-dihydro-1h-1,3,2-benzodiazaborole
CAS No.:6962-84-1
Molecular Formula:C16H13 B N2
Molecular Weight:244.104
Hs Code.:2934999090
NSC Number:54027
DSSTox Substance ID:DTXSID50288078
Nikkaji Number:J3.329.423I
Wikidata:Q82024353
Mol file:6962-84-1.mol

Synonyms:6962-84-1;2-(naphthalen-1-yl)-2,3-dihydro-1h-1,3,2-benzodiazaborole;NSC54027;DTXSID50288078;NSC-54027

Suppliers and Price of 2-(Naphthalen-1-yl)-2,3-dihydro-1h-1,3,2-benzodiazaborole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 2-(Naphthalen-1-yl)-2,3-dihydro-1h-1,3,2-benzodiazaborole

Chemical Property:

Vapor Pressure:2.7E-07mmHg at 25°C
Boiling Point:421°C at 760 mmHg
Flash Point:208.4°C
PSA：24.06000
Density:1.2g/cm³
LogP:3.34860
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:244.1171786
Heavy Atom Count:19
Complexity:308

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:B1(NC2=CC=CC=C2N1)C3=CC=CC4=CC=CC=C34

Technology Process of 2-(Naphthalen-1-yl)-2,3-dihydro-1h-1,3,2-benzodiazaborole

There total 3 articles about 2-(Naphthalen-1-yl)-2,3-dihydro-1h-1,3,2-benzodiazaborole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 13922-41-3
1-Naphthylboronic acid

: 95-54-5
1,2-diamino-benzene

: 6962-84-1
2-(1-naphthyl)-1,3-dihydro-1H-benzo[d]1,3,2-diazaborole

Guidance literature:: In toluene; byproducts: H2O; distg. the water with the solvent; filtering, recrystn. from benzene or CCl4;
DOI:10.1021/jo01037a021 DOI:10.1021/ja01520a024 DOI:10.1021/ja01553a023

Reference yield: 81.0%

: 90-11-9
1-Bromonaphthalene

: 95-54-5
1,2-diamino-benzene

: 6962-84-1
2-(1-naphthyl)-1,3-dihydro-1H-benzo[d]1,3,2-diazaborole

Guidance literature:: 1-Bromonaphthalene; With magnesium; In tetrahydrofuran; at 20 ℃;

With Trimethyl borate; In tetrahydrofuran; at -78 ℃;

1,2-diamino-benzene; In toluene; for 3h; Heating;
DOI:10.3762/bjoc.10.109