N-(4-Chlorophenyl)-3-phenylacrylamide

Base Information

• Chemical Name: N-(4-Chlorophenyl)-3-phenylacrylamide
• CAS No.: 53691-91-1
• Molecular Formula: C15H12ClNO
• Molecular Weight: 257.719
• Hs Code.: 2924299090
• Mol file: 53691-91-1.mol

Synonyms:N-(4-Chlorophenyl)-3-phenylacrylamide;N-(4-chlorophenyl)cinnamamide;N-(p-Chlor-phenyl)-cinamamid;N-(4-Chlorophenyl)-3-phenylpropenamide;

Chemical Property of N-(4-Chlorophenyl)-3-phenylacrylamide

Chemical Property:

• Vapor Pressure: 1.41E-08mmHg at 25°C
• Boiling Point: 458.1°Cat760mmHg
• Flash Point: 230.9°C
• PSA: 29.10000
• Density: 1.267g/cm³
• LogP: 4.06490

Purity/Quality:

99% ^*data from raw suppliers

N-(4-CHLOROPHENYL)-3-PHENYLACRYLAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-(4-Chlorophenyl)-3-phenylacrylamide

There total 14 articles about N-(4-Chlorophenyl)-3-phenylacrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

4-chloro-aniline (106-47-8) + Cinnamic acid (621-82-9) → N-(4-chlorophenyl)-3-phenylacrylamide (53691-91-1)

Guidance literature:

Cinnamic acid; With 2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine; In neat (no solvent); at 20 ℃; for 0.0166667h;

4-chloro-aniline; In neat (no solvent); at 20 ℃; for 0.166667h;

DOI:10.1016/j.tetlet.2013.07.033

Reference yield: 92.0%

cinnamoyl chloride (102-92-1,17082-09-6) + 4-chloro-aniline (106-47-8) → N-(4-chlorophenyl)-3-phenylacrylamide (53691-91-1)

Guidance literature:

With triethylamine; In ethyl acetate; at 0 - 20 ℃;

DOI:10.1039/b926560k

Reference yield: 92.0%

4-chloro-aniline (106-47-8) + hydrocinnamic acid chloride (645-45-4) → N-(4-chlorophenyl)-3-phenylacrylamide (53691-91-1)

Guidance literature:

With pyridine; dmap; In dichloromethane; at 0 ℃; for 1.25h;

DOI:10.1021/acsmedchemlett.7b00196

upstream raw materials:

cinnamoyl chloride

4-chloro-aniline

carbon monoxide

phenylacetylene

Downstream raw materials:

(E)-3-benzylidene-5-chloro-1,3-dihydro-indol-2-one

(Z)-3-benzylidene-5-chloroindolin-2-one

C₁₆H₁₁ClF₃NO

6-chloroquinolin-2(1H)-oney

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