3-(1H-1,2,3,4-Tetrazol-5-yl)-9H-carbazole

Base Information

• Chemical Name: 3-(1H-1,2,3,4-Tetrazol-5-yl)-9H-carbazole
• CAS No.: 503828-19-1
• Molecular Formula: C13H9N5
• Molecular Weight: 235.248
• Hs Code.: 2933990090
• Mol file: 503828-19-1.mol

Synonyms:3-(2H-tetrazol-5-yl)-2-trifluoromethyl-1-oxy-pyridine;3-(2H-tetrazol-5-yl)-9H-carbazole;Pyridine,3-(2H-tetrazol-5-yl)-2-(trifluoromethyl)-,1-oxide;

Chemical Property of 3-(1H-1,2,3,4-Tetrazol-5-yl)-9H-carbazole

Chemical Property:

• PSA: 70.25000
• LogP: 2.50120

Purity/Quality:

(2E)-But-2-enedioicacidbis(tert-butyl4-[(methyl-amino)methyl]piperidine-1-carboxylate) >95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 3-(1H-1,2,3,4-Tetrazol-5-yl)-9H-carbazole

There total 1 articles about 3-(1H-1,2,3,4-Tetrazol-5-yl)-9H-carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

(9H)-carbazole-3-carbonitrile (57102-93-9) → 3-(2H-tetrazol-5-yl)-9H-carbazole (503828-19-1)

Guidance literature:

With sodium azide; ammonium chloride; lithium chloride; In N,N-dimethyl-formamide; at 125 ℃; for 44h;

Reference yield:

3-(2H-tetrazol-5-yl)-9H-carbazole (503828-19-1) + trityl chloride (76-83-5) → 3-[2-(triphenylmethyl)-2H-tetrazol-5-yl]-9H-carbazole (720696-95-7)

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 18h;

Reference yield:

3-(2H-tetrazol-5-yl)-9H-carbazole (503828-19-1) + benzoyl chloride (98-88-4) → phenyl-[3-(2H-tetrazol-5-yl)-carbazol-9-yl]-methanone (720696-20-8)

Guidance literature:

3-(2H-tetrazol-5-yl)-9H-carbazole; With 2-chlorotrityl chloride polystyrene resin; N-ethyl-N,N-diisopropylamine; In DMF (N,N-dimethyl-formamide); dichloromethane; at 20 ℃; for 20h; 2-chlorotritylchloride resin

benzoyl chloride; With dmap; N-ethyl-N,N-diisopropylamine; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 48h;

With hydrogenchloride; ethanol; In tetrahydrofuran; diethyl ether; at 20 ℃; for 2h;

upstream raw materials:

(9H)-carbazole-3-carbonitrile

Downstream raw materials:

3-[2-(triphenylmethyl)-2H-tetrazol-5-yl]-9H-carbazole

phenyl-[3-(2H-tetrazol-5-yl)-carbazol-9-yl]-methanone

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