N-(2,6-dimethylphenyl)hydroxylamine

Base Information

• Chemical Name: N-(2,6-dimethylphenyl)hydroxylamine
• CAS No.: 3096-63-7
• Molecular Formula: C8H11 N O
• Molecular Weight: 137.181
• UNII: GQ8EDF3D00
• DSSTox Substance ID: DTXSID50184945
• Nikkaji Number: J534.611H
• Wikidata: Q83055889
• ChEMBL ID: CHEMBL3278068
• Mol file: 3096-63-7.mol

Synonyms:N-(2,6-dimethylphenyl)hydroxylamine;3096-63-7;Benzenamine, N-hydroxy-2,6-dimethyl-;2,6-Xylylhydroxylamine;CCRIS 5431;2,6-Dimethylphenylhydroxylamine;N-Hydroxy-2,6-dimethylbenzenamine;BRN 2081120;GQ8EDF3D00;Hydroxylamine, N-(2,6-xylyl)-;Benzenamine, N-hydroxy-2,6-dimethyl- (9CI);2-(hydroxyamino)-1,3-dimethylbenzene;starbld0038402;UNII-GQ8EDF3D00;hydroxy-2,6-dimethylaniline;n-hydroxy-2,6-dimethylaniline;SCHEMBL7603491;CHEMBL3278068;N-HYDROXY-2,6-XYLIDINE;DTXSID50184945;MFCD01721992;AKOS025395381;2M-328S;LS-77514

Chemical Property of N-(2,6-dimethylphenyl)hydroxylamine

Chemical Property:

• Vapor Pressure: 0.0327mmHg at 25°C
• Boiling Point: 232.5°Cat760mmHg
• Flash Point: 102.7°C
• Density: 1.12g/cm³
• XLogP3: 2.1
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 137.084063974
• Heavy Atom Count: 10
• Complexity: 95.4

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=C(C(=CC=C1)C)NO

Technology Process of N-(2,6-dimethylphenyl)hydroxylamine

There total 5 articles about N-(2,6-dimethylphenyl)hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2,6-dimethylnitrobenzene (81-20-9) → N-(2,6-dimethylphenyl)hydroxylamine (3096-63-7)

Guidance literature:

With hydrazine hydrate; at 85 ℃; for 1h;

DOI:10.1016/j.mcat.2021.111836

Reference yield:

2,6-dimethylnitrobenzene (81-20-9) → 1,2-bis(2,6-dimethylphenyl)diazene oxide (51284-70-9,80101-88-8) + N-(2,6-dimethylphenyl)hydroxylamine (3096-63-7) + 2,6-dimethylaniline (87-62-7)

Guidance literature:

Reference yield:

→ N-(2,6-dimethylphenyl)hydroxylamine (3096-63-7)

Guidance literature:

With potassium hydroxide; zinc;

upstream raw materials:

2,6-dimethylnitrobenzene

2,4-dimethyl-1,3,5-trinitrobenzene

Downstream raw materials:

4-methoxy-2,6-dimethylaniline

3,5-dimethyl-4-aminophenol

2,6-dimethylnitrosobenzene

2,6,2',6'-tetramethyl-4,4'-oxy-di-aniline