tris(2-carboxaldehyde)triphenylphosphine

Base Information

Chemical Name:tris(2-carboxaldehyde)triphenylphosphine
CAS No.:50777-83-8
Molecular Formula:C21H15O3P
Molecular Weight:346.31600
Hs Code.:
Mol file:50777-83-8.mol

Synonyms:2,2',2''-phosphinetriyltribenzaldehyde;Benzaldehyde,2,2',2''-phosphinidynetris;

Suppliers and Price of tris(2-carboxaldehyde)triphenylphosphine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Chemenu
2,2'',2''''-Phosphinetriyltribenzaldehyde 97%
1g
$ 309.00

Chemenu
2,2'',2''''-Phosphinetriyltribenzaldehyde 97%
5g
$ 926.00

Alichem
2,2',2''-Phosphinetriyltribenzaldehyde
5g
$ 1039.50

Alichem
2,2',2''-Phosphinetriyltribenzaldehyde
1g
$ 339.90

AK Scientific
2,2',2''-Phosphinetriyltribenzaldehyde
250mg
$ 212.00

Total 22 raw suppliers

Chemical Property of tris(2-carboxaldehyde)triphenylphosphine

Chemical Property:

Boiling Point:528.0±45.0 °C(Predicted)
PSA：64.80000
LogP:2.88230
Storage Temp.:under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

2,2'',2''''-Phosphinetriyltribenzaldehyde 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of tris(2-carboxaldehyde)triphenylphosphine

There total 4 articles about tris(2-carboxaldehyde)triphenylphosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 50777-81-6
tris-<2-(1,3-dioxolan-2-yl)phenyl>phosphine

: 50777-83-8
tris(2-carboxaldehyde)triphenylphosphine

Guidance literature:: With toluene-4-sulfonic acid; In acetone; for 25h; Heating;
DOI:10.1016/S0022-328X(96)06860-X

Reference yield:

: 34824-58-3
2-(2-bromophenyl)-1,3-dioxolan

: 50777-83-8
tris(2-carboxaldehyde)triphenylphosphine

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / 1.) Mg, iodine; 2.) PCl₃ / tetrahydrofuran / 1.) reflux, 1 h; 2.) -5 deg C; reflux, 24 h

2: 90 percent / 4-toluene sulfonic acid / acetone / 25 h / Heating

With iodine; toluene-4-sulfonic acid; magnesium; phosphorus trichloride; In tetrahydrofuran; acetone;
DOI:10.1016/S0022-328X(96)06860-X

Reference yield:

: 6630-33-7
ortho-bromobenzaldehyde

: 50777-83-8
tris(2-carboxaldehyde)triphenylphosphine

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / 4-toluene sulfonic acid / toluene / 12 h / Heating

2: 77 percent / 1.) Mg, iodine; 2.) PCl₃ / tetrahydrofuran / 1.) reflux, 1 h; 2.) -5 deg C; reflux, 24 h

3: 90 percent / 4-toluene sulfonic acid / acetone / 25 h / Heating

With iodine; toluene-4-sulfonic acid; magnesium; phosphorus trichloride; In tetrahydrofuran; acetone; toluene;
DOI:10.1016/S0022-328X(96)06860-X