Hydrazinecarbothioamide, 2-[(2-hydroxy-3-methoxyphenyl)methylene]-

Base Information

• Chemical Name: Hydrazinecarbothioamide, 2-[(2-hydroxy-3-methoxyphenyl)methylene]-
• CAS No.: 51146-75-9
• Molecular Formula: C9H11N3O2S
• Molecular Weight: 225.271
• Mol file: 51146-75-9.mol

Synonyms:

Chemical Property of Hydrazinecarbothioamide, 2-[(2-hydroxy-3-methoxyphenyl)methylene]-

Chemical Property:

Purity/Quality:

98%Min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Hydrazinecarbothioamide, 2-[(2-hydroxy-3-methoxyphenyl)methylene]-

There total 3 articles about Hydrazinecarbothioamide, 2-[(2-hydroxy-3-methoxyphenyl)methylene]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

3-methoxy-2-hydroxybenzaldehyde (148-53-8) + thiosemicarbazide (79-19-6) → 3-methoxysalicylaldehydethiosemicarbazone (51146-75-9)

Guidance literature:

With acetic acid; In methanol; for 3h; Reflux;

DOI:10.1016/j.molstruc.2012.12.061

Reference yield:

3-methoxy-2-hydroxybenzaldehyde (148-53-8) + thiosemicarbazide (79-19-6) → C9H11N3O2S (51146-75-9)

Guidance literature:

In ethanol; water;

DOI:10.1080/10426507.2012.717144

Reference yield:

→ 3-methoxysalicylaldehydethiosemicarbazone (51146-75-9)

Guidance literature:

/BRN= 471913/, Thiosemicarbazid;

upstream raw materials:

3-methoxy-2-hydroxybenzaldehyde

thiosemicarbazide

Downstream raw materials:

C₁₉H₁₄ClN₃O₄S

[Ni(Msal-tsc)(PPh₃)]Cl

Refernces

Synthesis, characterization and antimicrobial activity of some transition metal complexes of N-(5-chloro-2-hydroxyphenyl)-3-methoxy-salicylaldimine

10.4314/bcse.v29i1.6

The study focuses on the synthesis, characterization, and antimicrobial activity of transition metal complexes derived from N-(5-chloro-2-hydroxyphenyl)-3-methoxy-salicylaldimine (H2L), an ONO type tridentate ligand. The complexes of Cr(III), Fe(II), Fe(III), Co(II), Ni(II), Cu(II), and Zn(II) were prepared and characterized using various analytical techniques including elemental analysis, magnetic moment measurements, molar conductivity, thermogravimetric analysis (TGA), nuclear magnetic resonance (NMR), infrared (IR), ultraviolet-visible (UV-vis), and electrospray ionization-mass spectrometry (ESI-MS). The research revealed that all complexes, except for [Zn(L)(H2O)2], are paramagnetic and mostly adopt octahedral geometries, with the exception of Zn(II) and Fe(III) which exhibit five coordination geometries and Cu(II) which has a four-coordinated dimeric structure with acetato bridging. The antimicrobial activities of these complexes were tested against six bacterial strains and Candida albicans as a fungal strain, with Ni(II) and Co(II) complexes showing significant selective activity against S. epidermidis and C. albicans, and the Cr(III) complex displaying antibacterial activity against S. epidermidis, while the Zn(II) complex showed antifungal activity against C. albicans. The ligand itself did not exhibit any antimicrobial activity.

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