Carbonothioic dihydrazide, [(3-hydroxyphenyl)methylene]-

Base Information

• Chemical Name: Carbonothioic dihydrazide, [(3-hydroxyphenyl)methylene]-
• CAS No.: 51236-58-9
• Molecular Formula: C8H10N4OS
• Molecular Weight: 210.26
• Mol file: 51236-58-9.mol

Synonyms:

Chemical Property of Carbonothioic dihydrazide, [(3-hydroxyphenyl)methylene]-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Carbonothioic dihydrazide, [(3-hydroxyphenyl)methylene]-

There total 1 articles about Carbonothioic dihydrazide, [(3-hydroxyphenyl)methylene]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

Thiocarbohydrazide (2231-57-4) + meta-hydroxybenzaldehyde (100-83-4) → C8H10N4OS (51236-58-9)

Guidance literature:

With acetic acid; In ethanol; water; Reflux;

DOI:10.3184/174751911X13043447062703

Reference yield: 88.0%

C8H10N4OS (51236-58-9) + methyl 3,12-dioxo-5β-cholan-24-oate (1174-86-3,60103-18-6,28057-90-1) → C33H46N4O4S

Guidance literature:

With aluminum oxide; acetic acid; for 0.075h; Microwave irradiation;

DOI:10.3184/174751911X12995267948561

Reference yield: 82.0%

C8H10N4OS (51236-58-9) + methyl 3,7-dioxocholan-24-oate (7753-72-2) → methyl (5β)-3-[2-[[(3-hydroxyphenylideneamine)amino]thioxomethyl]hydrazinylidene]-7-oxocholan-24-oate

Guidance literature:

With hydrogenchloride; aluminum oxide; In neat (no solvent); for 0.116667h; Microwave irradiation;

DOI:10.1016/j.crci.2013.05.009

upstream raw materials:

Thiocarbohydrazide

meta-hydroxybenzaldehyde