Tert-butyl 3-phenylprop-2-ynylcarbamate

Base Information

Chemical Name:Tert-butyl 3-phenylprop-2-ynylcarbamate
CAS No.:512785-77-2
Molecular Formula:C14H17NO2
Molecular Weight:231.294
Hs Code.:
DSSTox Substance ID:DTXSID80457290
Nikkaji Number:J1.887.991C
Wikidata:Q82280082

Synonyms:512785-77-2;tert-butyl 3-phenylprop-2-ynylcarbamate;tert-Butyl (3-phenylprop-2-yn-1-yl)carbamate;tert-butyl N-(3-phenylprop-2-yn-1-yl)carbamate;Tert-butyl N-(3-phenylprop-2-ynyl)carbamate;SCHEMBL21881992;DTXSID80457290;MFCD11505628;t-Butyl 3-phenylprop-2-ynylcarbamate;AKOS030572012;AB22351;AS-44627;CS-0346594;EN300-40850;tert-Butyl(3-phenylprop-2-yn-1-yl)carbamate;1-Phenyl-3-(tert-butoxycarbonylamino)-1-propyne;Z414843308

Suppliers and Price of Tert-butyl 3-phenylprop-2-ynylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
TERT-BUTYL 3-PHENYLPROP-2-YNYLCARBAMATE 95.00%
5G
$ 1928.08

American Custom Chemicals Corporation
TERT-BUTYL 3-PHENYLPROP-2-YNYLCARBAMATE 95.00%
2.5G
$ 1473.14

American Custom Chemicals Corporation
TERT-BUTYL 3-PHENYLPROP-2-YNYLCARBAMATE 95.00%
1G
$ 983.52

Total 1 raw suppliers

Chemical Property of Tert-butyl 3-phenylprop-2-ynylcarbamate

Chemical Property:

PSA：41.82000
LogP:2.76720
XLogP3:2.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:231.125928785
Heavy Atom Count:17
Complexity:310

Purity/Quality:

99% ^*data from raw suppliers

TERT-BUTYL 3-PHENYLPROP-2-YNYLCARBAMATE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)OC(=O)NCC#CC1=CC=CC=C1

Technology Process of Tert-butyl 3-phenylprop-2-ynylcarbamate

There total 5 articles about Tert-butyl 3-phenylprop-2-ynylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 591-50-4
iodobenzene

: 92136-39-5
N-tert-Butoxycarbonyl-1-amino-3-propyne

: 512785-77-2
(3-phenyl-prop-2-ynyl)-carbamic acid tert-butyl ester

Guidance literature:: With copper(l) iodide; diethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In diethyl ether; at 35 ℃; for 2h;
DOI:10.1002/adsc.200404046

Reference yield: 83.0%

: 92136-39-5
N-tert-Butoxycarbonyl-1-amino-3-propyne

: 98-80-6
phenylboronic acid

: 512785-77-2
(3-phenyl-prop-2-ynyl)-carbamic acid tert-butyl ester

Guidance literature:: With pyridine; copper(I) oxide; methanol; In chloroform; at 25 ℃; for 36h; under 760.051 Torr;
DOI:10.1002/adsc.200900723

Reference yield: 76.0%

: 4530-20-5
BOC-glycine

: 1-Phenylethynyl-1H-1λ³-benzo[d][1,2]iodoxol-3-one

: 512785-77-2
(3-phenyl-prop-2-ynyl)-carbamic acid tert-butyl ester

Guidance literature:: With [4,4′-bis(1,1-dimethylethyl)-2,2′-bipyridine-N1,N1′]bis{3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-κN]phenyl-κC}iridium(III) hexafluorophosphate; caesium carbonate; In dichloromethane; at 20 ℃; for 4h; Molecular sieve; Irradiation; Schlenk technique;
DOI:10.1002/anie.201504559