2-allyl-N-tosylaniline

Base Information

Chemical Name:2-allyl-N-tosylaniline
CAS No.:51315-69-6
Molecular Formula:C16H17NO2S
Molecular Weight:287.382
Hs Code.:
DSSTox Substance ID:DTXSID90409265
Nikkaji Number:J744.699C
Wikidata:Q82215018

Synonyms:51315-69-6;2-allyl-N-tosylaniline;ST51007153;SCHEMBL8419064;DTXSID90409265;AKOS024371006

Suppliers and Price of 2-allyl-N-tosylaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 0 raw suppliers

Chemical Property of 2-allyl-N-tosylaniline

Chemical Property:

XLogP3:3.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:287.09799996
Heavy Atom Count:20
Complexity:405

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)NC2=CC=CC=C2CC=C

Technology Process of 2-allyl-N-tosylaniline

There total 10 articles about 2-allyl-N-tosylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 32704-22-6
2-allyl-phenylamine

: 98-59-9
p-toluenesulfonyl chloride

: 51315-69-6
N-tosyl-o-allylaniline

Guidance literature:: With pyridine; In chloroform; at 0 - 20 ℃;
DOI:10.1002/chem.201001656

Reference yield: 82.0%

: 32704-22-6
2-allyl-phenylamine

: 104-15-4
toluene-4-sulfonic acid

: 51315-69-6
N-tosyl-o-allylaniline

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.3390/molecules25051233

Reference yield:

: 589-09-3
N-allyl-N-phenylamine

: 51315-69-6
N-tosyl-o-allylaniline

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / BF₃*Et₂O / xylene / 2 h / 180 °C

2: 90 percent / pyridine / CH₂Cl₂ / 0 - 20 °C

With pyridine; boron trifluoride diethyl etherate; In dichloromethane; xylene; 1: aza-Claisen rearrangement;
DOI:10.1021/jo061486q