2-Dodecanone, 1-(phenylmethoxy)-

Base Information

Chemical Name:2-Dodecanone, 1-(phenylmethoxy)-
CAS No.:515828-17-8
Molecular Formula:C19H30O2
Molecular Weight:290.446
Hs Code.:

Synonyms:

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Chemical Property of 2-Dodecanone, 1-(phenylmethoxy)-

Chemical Property:

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Technology Process of 2-Dodecanone, 1-(phenylmethoxy)-

There total 3 articles about 2-Dodecanone, 1-(phenylmethoxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109538-39-8
1-O-benzyl-2-hydroxy-dodecane

: 515828-17-8
1-O-benzyloxy-2-oxo-dodecane

Guidance literature:: With phosphoric acid; dicyclohexyl-carbodiimide; In dimethyl sulfoxide; at 20 ℃; for 4h;
DOI:10.1021/ja029362s

Reference yield:

: 2855-19-8
Decyl-oxiran

: 515828-17-8
1-O-benzyloxy-2-oxo-dodecane

Guidance literature:: Multi-step reaction with 3 steps

1: NaHCO₃ / 1-methyl-pyrrolidin-2-one; H₂O / 24 h / 130 °C

2: 85 percent / dibutyltin oxide

3: orthophosphoric acid; DCC / dimethylsulfoxide / 4 h / 20 °C

With phosphoric acid; di(n-butyl)tin oxide; sodium hydrogencarbonate; dicyclohexyl-carbodiimide; In 1-methyl-pyrrolidin-2-one; water; dimethyl sulfoxide; 3: Pfitzner-Moffat oxidation;
DOI:10.1021/ja029362s

Reference yield:

: 1119-87-5
dodecane-1,2-diol

: 515828-17-8
1-O-benzyloxy-2-oxo-dodecane

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / dibutyltin oxide

2: orthophosphoric acid; DCC / dimethylsulfoxide / 4 h / 20 °C

With phosphoric acid; di(n-butyl)tin oxide; dicyclohexyl-carbodiimide; In dimethyl sulfoxide; 2: Pfitzner-Moffat oxidation;
DOI:10.1021/ja029362s