Phosphoric acid 2,2-difluoro-dodecyl ester (1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentahydroxy-cyclohexyl ester

Base Information

Chemical Name:Phosphoric acid 2,2-difluoro-dodecyl ester (1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentahydroxy-cyclohexyl ester
CAS No.:515828-31-6
Molecular Formula:C₁₈H₃₅F₂O₉P
Molecular Weight:464.441
Hs Code.:

Synonyms:Phosphoric acid 2,2-difluoro-dodecyl ester (1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentahydroxy-cyclohexyl ester

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Chemical Property of Phosphoric acid 2,2-difluoro-dodecyl ester (1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentahydroxy-cyclohexyl ester

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Technology Process of Phosphoric acid 2,2-difluoro-dodecyl ester (1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentahydroxy-cyclohexyl ester

There total 10 articles about Phosphoric acid 2,2-difluoro-dodecyl ester (1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentahydroxy-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Phosphoric acid 2,2-difluoro-dodecyl ester methyl ester (1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-methoxymethoxy-cyclohexyl ester

: 515828-31-6
Phosphoric acid 2,2-difluoro-dodecyl ester (1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentahydroxy-cyclohexyl ester

Guidance literature:: Phosphoric acid 2,2-difluoro-dodecyl ester methyl ester (1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-methoxymethoxy-cyclohexyl ester; With trimethylamine; at 50 ℃;

With boron trifluoride diethyl etherate; ethanethiol; at 20 ℃; for 1h; Further stages.;
DOI:10.1021/ja029362s

Reference yield:

: 515828-18-9
1-O-benzyloxy-2,2-difluorododecane

: 515828-31-6
Phosphoric acid 2,2-difluoro-dodecyl ester (1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentahydroxy-cyclohexyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: 99 percent / H₂/Pd

2.1: CHCl₃ / 0 - 20 °C

3.1: t-BuOOH / decane

4.1: trimethylamine / 50 °C

4.2: BF₃*Et₂O; EtSH / 1 h / 20 °C

With tert.-butylhydroperoxide; hydrogen; palladium; trimethylamine; In decane; chloroform;
DOI:10.1021/ja029362s

Reference yield:

: 515828-17-8
1-O-benzyloxy-2-oxo-dodecane

: 515828-31-6
Phosphoric acid 2,2-difluoro-dodecyl ester (1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentahydroxy-cyclohexyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: 80 percent / DAST / CH₂Cl₂ / 0 °C

2.1: 99 percent / H₂/Pd

3.1: CHCl₃ / 0 - 20 °C

4.1: t-BuOOH / decane

5.1: trimethylamine / 50 °C

5.2: BF₃*Et₂O; EtSH / 1 h / 20 °C

With tert.-butylhydroperoxide; hydrogen; palladium; 4,4'-diaminostilbene-2,2'-disulfonic acid; trimethylamine; In decane; dichloromethane; chloroform;
DOI:10.1021/ja029362s