Diethyl 4-oxo-4H-quinolizine-1,3-dicarboxylate

Base Information

Chemical Name:Diethyl 4-oxo-4H-quinolizine-1,3-dicarboxylate
CAS No.:54401-76-2
Molecular Formula:C15H15NO5
Molecular Weight:289.2833
Hs Code.:2918300090
NSC Number:96508
UNII:QI141362ZO
DSSTox Substance ID:DTXSID10202795
Nikkaji Number:J1.426.267I
Wikidata:Q83076112
ChEMBL ID:CHEMBL1566749
Mol file:54401-76-2.mol

Synonyms:Diethyl 4-oxo-4H-quinolizine-1,3-dicarboxylate;54401-76-2;diethyl 4-oxoquinolizine-1,3-dicarboxylate;1,3-Dicarboethoxy-4-quinolizone;QI141362ZO;NSC96508;NSC 96508;UNII-QI141362ZO;MLS000538212;NSC-96508;SMR000162689;NCIOpen2_007045;Oprea1_002113;cid_262620;CHEMBL1566749;SCHEMBL10796863;BDBM51687;DTXSID10202795;HMS2311O21;NCGC00247257-01;1,3-diethoxycarbonyl-4H-quinolizin-4-one;AC-907/25000244;diethyl 4-oxidanylidenequinolizine-1,3-dicarboxylate;4-ketoquinolizine-1,3-dicarboxylic acid diethyl ester;4-oxoquinolizine-1,3-dicarboxylic acid diethyl ester;4-oxo-5H-quinolizine-1,3-dicarboxylic acid diethyl ester;4H-Quinolizine-1,3-dicarboxylic acid, 4-oxo-, diethyl ester;4H-QUINOLIZINE-1,3-DICARBOXYLIC ACID, 4-OXO-, 1,3-DIETHYL ESTER

Suppliers and Price of Diethyl 4-oxo-4H-quinolizine-1,3-dicarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 10 raw suppliers

Chemical Property of Diethyl 4-oxo-4H-quinolizine-1,3-dicarboxylate

Chemical Property:

Vapor Pressure:1.58E-09mmHg at 25°C
Refractive Index:1.584
Boiling Point:484.1 °C at 760 mmHg
Flash Point:246.6 °C
PSA：74.08000
Density:1.3 g/cm³
LogP:1.65290
XLogP3:1.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:6
Exact Mass:289.09502258
Heavy Atom Count:21
Complexity:610

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C1=CC(=C2C=CC=CN2C1=O)C(=O)OCC

Technology Process of Diethyl 4-oxo-4H-quinolizine-1,3-dicarboxylate

There total 7 articles about Diethyl 4-oxo-4H-quinolizine-1,3-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: diethyl 1,6-diallyl-2-oxo-1,2-dihydropyridine-3,5-dicarboxylate

: C₁₅H₁₇NO₅

: 54401-76-2
diethyl 4-oxo-4H-quinolizine-1,3-dicarboxylate

Guidance literature:: diethyl 1,6-diallyl-2-oxo-1,2-dihydropyridine-3,5-dicarboxylate; With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;

With palladium 10% on activated carbon; at 150 ℃; Inert atmosphere;
DOI:10.1002/ejoc.201402648