Magnesium bromide (2,5-difluorophenyl)methanide (1/1/1)

Base Information

Chemical Name:Magnesium bromide (2,5-difluorophenyl)methanide (1/1/1)
CAS No.:522651-57-6
Molecular Formula:C7H5BrF2Mg
Molecular Weight:231.32000
Hs Code.:2840209090
DSSTox Substance ID:DTXSID40381042
Mol file:522651-57-6.mol

Synonyms:Magnesium bromide (2,5-difluorophenyl)methanide (1/1/1);magnesium;1,4-difluoro-2-methanidylbenzene;bromide;DTXSID40381042

Suppliers and Price of Magnesium bromide (2,5-difluorophenyl)methanide (1/1/1)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Rieke Metals
2,5-Difluorobenzylmagnesiumbromide
50mL
$ 283.00

American Custom Chemicals Corporation
2,5-DIFLUOROBENZYLMAGNESIUM BROMIDE 95.00%
500ML
$ 4966.50

American Custom Chemicals Corporation
2,5-DIFLUOROBENZYLMAGNESIUM BROMIDE 95.00%
200ML
$ 2772.00

American Custom Chemicals Corporation
2,5-DIFLUOROBENZYLMAGNESIUM BROMIDE 95.00%
100ML
$ 2598.75

Total 5 raw suppliers

Chemical Property of Magnesium bromide (2,5-difluorophenyl)methanide (1/1/1)

Chemical Property:

PSA：0.00000
LogP:3.12610
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:0
Exact Mass:229.93931
Heavy Atom Count:11
Complexity:92.9

Purity/Quality:

98% ^*data from raw suppliers

2,5-Difluorobenzylmagnesiumbromide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:F

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:[CH2-]C1=C(C=CC(=C1)F)F.[Mg+2].[Br-]

Technology Process of Magnesium bromide (2,5-difluorophenyl)methanide (1/1/1)

There total 1 articles about Magnesium bromide (2,5-difluorophenyl)methanide (1/1/1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85117-99-3
2-(bromomethyl)-1,4-difluorobenzene

: 522651-57-6
2,5-difluorobenzylmagnesium bromide

Guidance literature:: With iodine; magnesium; In diethyl ether; for 1.66667h; Heating / reflux;

Reference yield:

: 3612-20-2
1-phenylmethyl-4-piperidone

: 522651-57-6
2,5-difluorobenzylmagnesium bromide

: 644967-96-4
1-benzyl-4-(2,5-difluorobenzyl)piperidin-4-ol

Guidance literature:: 1-phenylmethyl-4-piperidone; 2,5-difluorobenzylmagnesium bromide; In diethyl ether; at 20 ℃;

With ammonium chloride; In diethyl ether; water; at 20 ℃;

Reference yield:

: 1131872-72-4
4-{(R)-3-[1-(3-isopropyl-[1,2,4]oxadiazol-5-yl)piperidin-4-yl]butoxy}-benzaldehyde

: 522651-57-6
2,5-difluorobenzylmagnesium bromide

: 1131870-08-0
(R)-2-(2,5-difluorophenyl)-1-(4-{(R)-3-[1-(3-isopropyl-[1,2,4]oxadiazol-5-yl)-piperidin-4-yl]butoxy}phenyl)ethylamine

Guidance literature:: 4-{(R)-3-[1-(3-isopropyl-[1,2,4]oxadiazol-5-yl)piperidin-4-yl]butoxy}-benzaldehyde; With lithium hexamethyldisilazane; In tetrahydrofuran; at 0 ℃; for 0.5h;

2,5-difluorobenzylmagnesium bromide; In tetrahydrofuran; at 20 ℃; for 3h;

With water; ammonium chloride; In tetrahydrofuran;