Stannane, trimethyl(4-nitrophenyl)-

Base Information

Chemical Name:Stannane, trimethyl(4-nitrophenyl)-
CAS No.:52323-94-1
Molecular Formula:C9H13NO2Sn
Molecular Weight:285.918
Hs Code.:
DSSTox Substance ID:DTXSID20433513
Wikidata:Q82247679
Mol file:52323-94-1.mol

Synonyms:Stannane, trimethyl(4-nitrophenyl)-;52323-94-1;trimethyl(4-nitrophenyl)tin;SCHEMBL5952091;DTXSID20433513;MCNXUQBOSODMEE-UHFFFAOYSA-N

Suppliers and Price of Stannane, trimethyl(4-nitrophenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of Stannane, trimethyl(4-nitrophenyl)-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:286.996831
Heavy Atom Count:13
Complexity:187

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Sn](C)(C)C1=CC=C(C=C1)[N+](=O)[O-]

Technology Process of Stannane, trimethyl(4-nitrophenyl)-

There total 7 articles about Stannane, trimethyl(4-nitrophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 636-98-6
p-nitrobenzene iodide

: 661-69-8
hexamethyldistannane

: 52323-94-1
trimethyl(4-nitrophenyl)stannane

Guidance literature:: dichloro bis(acetonitrile) palladium(II); In N,N-dimethyl-formamide; byproducts: (CH3)3SnI; Me6Sn2, p-NO2C6H4I dissolved in DMF in a flask, catalyst added with stirring, reacted for 5 min at 20°C; water added, extracted with ether, extracts filtered, washed with water, dried with Na2SO4, chromy.(silica gel, hexane/ether 2:1);

Reference yield: 86.0%

: 661-69-8
hexamethyldistannane

: 100-01-6,104810-17-5
4-nitro-aniline

: 52323-94-1
trimethyl(4-nitrophenyl)stannane

Guidance literature:: With tert.-butylnitrite; toluene-4-sulfonic acid; In 1,2-dichloro-ethane; at 0 ℃; for 4h; Inert atmosphere;
DOI:10.1002/anie.201304579