2-Naphthalenol, 1,2,3,4-tetrahydro-, methanesulfonate

Base Information

Chemical Name:2-Naphthalenol, 1,2,3,4-tetrahydro-, methanesulfonate
CAS No.:52802-20-7
Molecular Formula:C11H14O3S
Molecular Weight:226.296
Hs Code.:
Mol file:52802-20-7.mol

Synonyms:2-methylsulphonyloxytetralin;methanesulphonic acid 1,2,3,4-tetrahydro-naphthalen-2-yl ester;Methanesulfonic acid 1,2,3,4-tetrahydro-naphthalen-2-yl ester;1,2,3,4-tetrahydro-2-naphthalenyl methanesulfonate;β-Tetralol-mesylat;

Suppliers and Price of 2-Naphthalenol, 1,2,3,4-tetrahydro-, methanesulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Alichem
1,2,3,4-Tetrahydronaphthalen-2-ylmethanesulfonate
1g
$ 438.00

Total 0 raw suppliers

Chemical Property of 2-Naphthalenol, 1,2,3,4-tetrahydro-, methanesulfonate

Chemical Property:

PSA：51.75000
LogP:2.60090

Purity/Quality:: 1,2,3,4-Tetrahydronaphthalen-2-ylmethanesulfonate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Naphthalenol, 1,2,3,4-tetrahydro-, methanesulfonate

There total 3 articles about 2-Naphthalenol, 1,2,3,4-tetrahydro-, methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 530-91-6
1,2,3,4-tetrahydronaphthalen-2 ol

: 124-63-0
methanesulfonyl chloride

: 52802-20-7
1,2,3,4-tetrahydronaphthalen-2-yl methanesulfonate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; for 0.166667h; Inert atmosphere;
DOI:10.1016/j.ejmech.2009.09.020

Reference yield:

: 530-93-8
1,2,3,4-tetrahydronaphthalen-2-one

: 52802-20-7
1,2,3,4-tetrahydronaphthalen-2-yl methanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate; methanol / 1 h / 0 - 20 °C

2: triethylamine / dichloromethane / 2 h / 0 °C

With methanol; sodium tetrahydroborate; triethylamine; In dichloromethane;