2,3,6-Trimethoxy-5-methyl-5,6-dihydro-9H-benzo[c][1,3]dioxolo[4,5-j]phenanthridine

Base Information

Chemical Name:2,3,6-Trimethoxy-5-methyl-5,6-dihydro-9H-benzo[c][1,3]dioxolo[4,5-j]phenanthridine
CAS No.:51116-34-8
Molecular Formula:C22H21NO5
Molecular Weight:379.4058
Hs Code.:
NSC Number:172620
DSSTox Substance ID:DTXSID40305920

Synonyms:51116-34-8;NSC172620;SCHEMBL11742857;DTXSID40305920;NSC-172620;Benzo[c][1,5-j]phenanthridine, 5,6-dihydro-2,3,6-trimethoxy-5-methyl-;2,3,6-Trimethoxy-5-methyl-5,6-dihydro-9H-benzo[c][1,3]dioxolo[4,5-j]phenanthridine

Suppliers and Price of 2,3,6-Trimethoxy-5-methyl-5,6-dihydro-9H-benzo[c][1,3]dioxolo[4,5-j]phenanthridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 2,3,6-Trimethoxy-5-methyl-5,6-dihydro-9H-benzo[c][1,3]dioxolo[4,5-j]phenanthridine

Chemical Property:

Vapor Pressure:1.43E-12mmHg at 25°C
Boiling Point:560°Cat760mmHg
Flash Point:165.6°C
Density:1.36g/cm³
XLogP3:4.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:3
Exact Mass:379.14197277
Heavy Atom Count:28
Complexity:561

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN1C(C2=CC3=C(C=C2C4=C1C5=CC(=C(C=C5C=C4)OC)OC)OCO3)OC

Technology Process of 2,3,6-Trimethoxy-5-methyl-5,6-dihydro-9H-benzo[c][1,3]dioxolo[4,5-j]phenanthridine

There total 4 articles about 2,3,6-Trimethoxy-5-methyl-5,6-dihydro-9H-benzo[c][1,3]dioxolo[4,5-j]phenanthridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51116-28-0
2,3-dimethoxy-4b,11b,12,13-tetrahydro-benzo[c][1,3]dioxolo[4,5-j]phenanthridine

: 51116-34-8
2,3,6-trimethoxy-5-methyl-5,6-dihydro-benzo[c][1,3]dioxolo[4,5-j]phenanthridine

Guidance literature:: Multi-step reaction with 3 steps

1: Pd-C

2: xylene; nitrobenzene

3: aq. NH₃

With ammonium hydroxide; palladium on activated charcoal; In nitrobenzene; xylene;
DOI:10.1002/jhet.5570100532

Reference yield:

: 51116-27-9
N-(2-benzo[1,3]dioxol-5-yl-6,7-dimethoxy-1,2,3,4-tetrahydro-naphthalen-1-yl)-formamide

: 51116-34-8
2,3,6-trimethoxy-5-methyl-5,6-dihydro-benzo[c][1,3]dioxolo[4,5-j]phenanthridine

Guidance literature:: Multi-step reaction with 4 steps

1: POCl₃ / toluene

2: Pd-C

3: xylene; nitrobenzene

4: aq. NH₃

With ammonium hydroxide; trichlorophosphate; palladium on activated charcoal; In nitrobenzene; toluene; xylene;
DOI:10.1002/jhet.5570100532

Reference yield:

: 51116-29-1
norallonitidine

: 51116-34-8
2,3,6-trimethoxy-5-methyl-5,6-dihydro-benzo[c][1,3]dioxolo[4,5-j]phenanthridine

Guidance literature:: Multi-step reaction with 2 steps

1: xylene; nitrobenzene

2: aq. NH₃

With ammonium hydroxide; In nitrobenzene; xylene;
DOI:10.1002/jhet.5570100532