Spiro(5H-dibenzo(a,d)cycloheptene-5,5'-oxazolidine)-2',4'-dione, 10,11-dihydro-

Base Information

• Chemical Name: Spiro(5H-dibenzo(a,d)cycloheptene-5,5'-oxazolidine)-2',4'-dione, 10,11-dihydro-
• CAS No.: 64036-60-8
• Molecular Formula: C₁₇H₁₃NO₃
• Molecular Weight: 279.295
• Hs Code.: 2934999090
• DSSTox Substance ID: DTXSID20214021
• Nikkaji Number: J87.091I
• Wikidata: Q83089729
• Mol file: 64036-60-8.mol

Synonyms:64036-60-8;Spiro(5H-dibenzo(a,d)cycloheptene-5,5'-oxazolidine)-2',4'-dione, 10,11-dihydro-;BRN 1014999;Spiro(dibenzo(a,d)(1,4)cycloheptadiene-5,5'-oxazolidine)-2',4'-dione;DTXSID20214021

Chemical Property of Spiro(5H-dibenzo(a,d)cycloheptene-5,5'-oxazolidine)-2',4'-dione, 10,11-dihydro-

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 58.89000
• Density: 1.38g/cm³
• LogP: 2.57110
• XLogP3: 3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 0
• Exact Mass: 279.08954328
• Heavy Atom Count: 21
• Complexity: 437

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CC2=CC=CC=C2C3(C4=CC=CC=C41)C(=O)NC(=O)O3

Technology Process of Spiro(5H-dibenzo(a,d)cycloheptene-5,5'-oxazolidine)-2',4'-dione, 10,11-dihydro-

There total 2 articles about Spiro(5H-dibenzo(a,d)cycloheptene-5,5'-oxazolidine)-2',4'-dione, 10,11-dihydro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Methyl 10,11-dihydro-5-hydroxydibenzo[a,d]cycloheptene-5-carboxylate (10541-20-5) + urea (57-13-6) → Spiro<1.4>cycloheptadien-5,5'-oxazolidin-2',4'-dion (64036-60-8)

Guidance literature:

With sodium; In ethanol;

DOI:10.1021/jm00334a009

Reference yield:

→ Spiro<1.4>cycloheptadien-5,5'-oxazolidin-2',4'-dion (64036-60-8)

Guidance literature:

Methylester III, CO(NH2)2/A.;

upstream raw materials:

Methyl 10,11-dihydro-5-hydroxydibenzo[a,d]cycloheptene-5-carboxylate

urea

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