1H-Imidazole-5-methanol, 1-[(4-methylphenyl)sulfonyl]-, acetate (ester)

Base Information

• Chemical Name: 1H-Imidazole-5-methanol, 1-[(4-methylphenyl)sulfonyl]-, acetate (ester)
• CAS No.: 52961-34-9
• Molecular Formula: C13H14N2O4S
• Molecular Weight: 294.32600

Synonyms:1-Tosyl-4-acetoxymethylimidazol;Acetic acid 3-(toluene-4-sulfonyl)-3H-imidazol-4-ylmethyl ester;

Chemical Property of 1H-Imidazole-5-methanol, 1-[(4-methylphenyl)sulfonyl]-, acetate (ester)

Chemical Property:

• Boiling Point: 473.4±47.0 °C(Predicted)
• PSA: 86.64000
• Density: 1.32±0.1 g/cm3(Predicted)
• LogP: 2.57240

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1H-Imidazole-5-methanol, 1-[(4-methylphenyl)sulfonyl]-, acetate (ester)

There total 2 articles about 1H-Imidazole-5-methanol, 1-[(4-methylphenyl)sulfonyl]-, acetate (ester) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

{1-[(4-methylphenyl)sulfonyl]-1H-imidazol-2-yl}methanol (52961-33-8) → 5-acetoxymethyl-1-tosylimidazole (52961-34-9)

Guidance literature:

With acetic anhydride; triethylamine; In chloroform; ethyl acetate;

Reference yield:

→ 5-acetoxymethyl-1-tosylimidazole (52961-34-9)

Guidance literature:

1-Tosyl-4-hydroxymethylimidazol 2, Acetanhydrid;

DOI:10.1080/00021369.1974.10861291

Reference yield:

2-ethoxy-1,1,1-trifluoro-3-(1-tosyl-5-imidazolyl)prop-2-ene + ethyl trifluoroacetate, (383-63-1) + 5-acetoxymethyl-1-tosylimidazole (52961-34-9) → trifluoromethyl 1-tosylimidazol-5-ylmethyl ketone

Guidance literature:

With sulfuric acid; sodium; triphenylphosphine; ferric nitrate; In ammonia; water; benzene;

upstream raw materials:

{1-[(4-methylphenyl)sulfonyl]-1H-imidazol-2-yl}methanol

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