2,3,4-TRIMETHOXY-6-NITROBENZALDEHYDE

Base Information

• Chemical Name: 2,3,4-TRIMETHOXY-6-NITROBENZALDEHYDE
• CAS No.: 52978-83-3
• Molecular Formula: C10H11NO6
• Molecular Weight: 241.2
• Hs Code.: 2913000090
• Mol file: 52978-83-3.mol

Synonyms:2,3,4-TRIMETHOXY-6-NITROBENZALDEHYDE

Chemical Property of 2,3,4-TRIMETHOXY-6-NITROBENZALDEHYDE

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Refractive Index: 1.558
• Boiling Point: 425.078 °C at 760 mmHg
• Flash Point: 203.646 °C
• PSA: 90.58000
• Density: 1.304 g/cm³
• LogP: 1.95630

Purity/Quality:

99% ^*data from raw suppliers

2,3,4-Trimethoxy-6-nitrobenzaldehyde ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3,4-TRIMETHOXY-6-NITROBENZALDEHYDE

There total 2 articles about 2,3,4-TRIMETHOXY-6-NITROBENZALDEHYDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2,3,4-trimethoxybenzaldehyde (2103-57-3) → 2,3,4-trimethoxy-6-nitrobenzaldehyde (52978-83-3)

Guidance literature:

With nitric acid; acetic acid; at 0 ℃; for 0.5h;

DOI:10.1155/2018/9242616

Reference yield:

→ 2,3,4-trimethoxy-6-nitrobenzaldehyde (52978-83-3)

Guidance literature:

2,3,4-Trimethoxy-benzaldehyd, Nitriersaeure;

Reference yield: 100.0%

2,3,4-trimethoxy-6-nitrobenzaldehyde (52978-83-3) + vinyl magnesium bromide (1826-67-1) → 1-(6-nitro-2,3,4-trimethoxyphenyl)prop-2-en-1-ol (1445859-28-8)

Guidance literature:

In tetrahydrofuran; at -70 ℃; for 3.5h;

DOI:10.1016/j.bmc.2013.05.016

upstream raw materials:

2,3,4-trimethoxybenzaldehyde

Downstream raw materials:

2-hydroxymethyl-1-nitro-3,4,5-trimethoxybenzene

1-(2',3',4'-trimethoxyphenyl)-2-nitroprop-1-ene

5-[1-(2,3,4-Trimethoxy-6-nitro-phenyl)-meth-(E)-ylidene]-imidazolidine-2,4-dione

5-[1-(2,3,4-Trimethoxy-6-nitro-phenyl)-meth-(Z)-ylidene]-imidazolidine-2,4-dione

Refernces

• 1、 Barnes, Natalie G.,Nyandoro, Kudakwashe,Jin, Hanzhang,Macmillan, Derek. "Rapid access to Asp/Glu sidechain hydrazides as thioester precursors for peptide cyclization and glycosylation". supporting information. p. 1006 - 1009. Retrieved 2021/02/05.
• 2、 Carreras, Javier,Gopakumar, Gopinadhanpillai,Gu, Liangu,Gimeno, Ana,Linowski, Pawel,Petu?kova, Jekaterina,Thiel, Walter,Alcarazo, Manuel. "Polycationic ligands in gold catalysis: Synthesis and applications of extremely π-acidic catalysts". supporting information. p. 18815 - 18823. Retrieved 2014/01/06.