Technology Process of Benzeneethanamine, b-phenyl-b-2-propenyl-
There total 11 articles about Benzeneethanamine, b-phenyl-b-2-propenyl- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
diethyl ether;
at 0 - 20 ℃;
Inert atmosphere;
DOI:10.1021/acs.orglett.0c03090
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: n-BuLi; diisopropylamine / tetrahydrofuran; hexane / 2 h / -78 °C
1.2: hexane; tetrahydrofuran / -78 - 20 °C
2.1: 7.609 g / LiAlH4 / diethyl ether / 4 h / Heating
With
lithium aluminium tetrahydride; n-butyllithium; diisopropylamine;
In
tetrahydrofuran; diethyl ether; hexane;
DOI:10.1039/b518360j
- Guidance literature:
-
With
C27H40FeN2Si*C4H8O; Cyclopentamine;
In
toluene;
at 90 ℃;
for 24h;
Temperature;
Sealed tube;
Inert atmosphere;
DOI:10.1002/chem.201804681
