Methanone, (2-azido-5-nitrophenyl)phenyl-

Base Information

• Chemical Name: Methanone, (2-azido-5-nitrophenyl)phenyl-
• CAS No.: 53879-06-4
• Molecular Formula: C13H8N4O3
• Molecular Weight: 268.232
• DSSTox Substance ID: DTXSID90458435
• Wikidata: Q82281704
• Mol file: 53879-06-4.mol

Synonyms:Methanone, (2-azido-5-nitrophenyl)phenyl-;53879-06-4;DTXSID90458435

Chemical Property of Methanone, (2-azido-5-nitrophenyl)phenyl-

Chemical Property:

• XLogP3: 4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 3
• Exact Mass: 268.05964013
• Heavy Atom Count: 20
• Complexity: 422

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C(=O)C2=C(C=CC(=C2)[N+](=O)[O-])N=[N+]=[N-]

Technology Process of Methanone, (2-azido-5-nitrophenyl)phenyl-

There total 3 articles about Methanone, (2-azido-5-nitrophenyl)phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2-amino-5-nitrobenzophenone (1775-95-7) → (2-azido-5-nitrophenyl)(phenyl)methanone (53879-06-4)

Guidance literature:

2-amino-5-nitrobenzophenone; With acetic acid; sodium nitrite; In water; at 0 ℃; for 1h;

With sodium azide; In water; for 1h;

Reference yield:

aqueous sodium nitrite + concentrated hydrochlorid acid + 2-amino-5-nitrobenzophenone (1775-95-7) → (2-azido-5-nitrophenyl)(phenyl)methanone (53879-06-4)

Guidance literature:

With sodium acetate; In (2S)-N-methyl-1-phenylpropan-2-amine hydrate; water; acetic acid; benzene;

Reference yield:

→ (2-azido-5-nitrophenyl)(phenyl)methanone (53879-06-4)

Guidance literature:

Amin, Diazotierg.;

upstream raw materials:

2-amino-5-nitrobenzophenone

Downstream raw materials:

5-nitro-3-phenyl-2,1-benzisoxazole

2-amino-5-nitrobenzophenone

C₁₄H₁₁N₅O₃