Benzamide, 2-amino-6-ethoxy-

Base Information

Chemical Name:Benzamide, 2-amino-6-ethoxy-
CAS No.:54166-99-3
Molecular Formula:C9H12N2O2
Molecular Weight:180.206
Hs Code.:

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Chemical Property of Benzamide, 2-amino-6-ethoxy-

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Technology Process of Benzamide, 2-amino-6-ethoxy-

There total 7 articles about Benzamide, 2-amino-6-ethoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 385-02-4
6-fluoro-2-nitrobenzoic acid

: 54166-99-3
2-amino-6-ethoxybenzamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 80 °C

2.1: sodium ethanolate / tetrahydrofuran / 2 h / 0 - 25 °C

3.1: sodium hydroxide; methanol / 18 h / 25 °C

4.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 0 - 25 °C / Inert atmosphere

4.2: 16 h / -30 - 25 °C

5.1: palladium 10% on activated carbon; hydrogen / methanol / 16 h / 40 °C / 775.74 Torr

With methanol; oxalyl dichloride; palladium 10% on activated carbon; hydrogen; sodium ethanolate; potassium carbonate; N,N-dimethyl-formamide; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;