2-(Benzenesulfinyl)-1,1-diphenylethanol

Base Information

Chemical Name:2-(Benzenesulfinyl)-1,1-diphenylethanol
CAS No.:23975-23-7
Molecular Formula:C20H18 O2 S
Molecular Weight:322.428
Hs Code.:
NSC Number:170764
DSSTox Substance ID:DTXSID70305433
Nikkaji Number:J2.886.966E
Mol file:23975-23-7.mol

Synonyms:23975-23-7;2-(benzenesulfinyl)-1,1-diphenylethanol;NSC170764;DTXSID70305433;NSC-170764

Suppliers and Price of 2-(Benzenesulfinyl)-1,1-diphenylethanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 2-(Benzenesulfinyl)-1,1-diphenylethanol

Chemical Property:

Vapor Pressure:2.8E-13mmHg at 25°C
Boiling Point:557.8°Cat760mmHg
Flash Point:291.2°C
Density:1.28g/cm³
XLogP3:3.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:322.10275099
Heavy Atom Count:23
Complexity:359

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(CS(=O)C2=CC=CC=C2)(C3=CC=CC=C3)O

Technology Process of 2-(Benzenesulfinyl)-1,1-diphenylethanol

There total 4 articles about 2-(Benzenesulfinyl)-1,1-diphenylethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 119-61-9
benzophenone

: [Li₂{CH₂S(O)(C₆H₅)}₂(N,N,N’,N’-tetramethylethylenediamine)₂]

: 23975-23-7
2-benzenesulfinyl-1,1-diphenylethanol

Guidance literature:: benzophenone; [Li₂{CH₂S(O)(C₆H₅)}₂(N,N,N’,N’-tetramethylethylenediamine)₂]; In diethyl ether; at -78 ℃;

at 20 ℃; for 1h;

With ammonium chloride; In water; at 0 ℃;
DOI:10.1039/c4dt02238f

Reference yield:

: 119-61-9
benzophenone

: methyllithium lithium bromide

: 65325-68-0
1-(monofluoromethyl sulfinyl)benzene

: 1193-82-4
racemic methyl phenyl sulfoxide

: 23975-23-7
2-benzenesulfinyl-1,1-diphenylethanol

: 337-72-4
2-fluoro-1,1-diphenylethan-1-ol

Guidance literature:: In diethyl ether; at -98 ℃; Inert atmosphere;
DOI:10.1021/jacs.7b07891

Reference yield:

: 1193-82-4
racemic methyl phenyl sulfoxide

: 23975-23-7
2-benzenesulfinyl-1,1-diphenylethanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: diethyl ether; hexane; pentane / 6 - 12 h / 20 °C / Schlenk technique; Inert atmosphere

2.1: diethyl ether / -78 °C

2.2: 1 h / 20 °C

2.3: 0 °C

In diethyl ether; hexane; pentane;
DOI:10.1039/c4dt02238f