Ethanone, 1-[2-hydroxy-4,6-dimethoxy-3-(phenylmethoxy)phenyl]-

Base Information

Chemical Name:Ethanone, 1-[2-hydroxy-4,6-dimethoxy-3-(phenylmethoxy)phenyl]-
CAS No.:54299-57-9
Molecular Formula:C₁₇H₁₈O₅
Molecular Weight:302.327
Hs Code.:

Synonyms:3-benzyloxy-2-hydroxy-4,6-dimethoxyacetophenone;Ethanone,1-[2-hydroxy-4,6-dimethoxy-3-(phenylmethoxy)phenyl];

Suppliers and Price of Ethanone, 1-[2-hydroxy-4,6-dimethoxy-3-(phenylmethoxy)phenyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethanone, 1-[2-hydroxy-4,6-dimethoxy-3-(phenylmethoxy)phenyl]-

Chemical Property:

Melting Point:95–97°C
PSA：64.99000
LogP:3.19100

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Ethanone, 1-[2-hydroxy-4,6-dimethoxy-3-(phenylmethoxy)phenyl]-

There total 4 articles about Ethanone, 1-[2-hydroxy-4,6-dimethoxy-3-(phenylmethoxy)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89456-13-3
2,3-bis(benzyloxy)-4,6-dimethoxyacetophenone

: 54299-57-9
3-benzyloxy-2-hydroxy-4,6-dimethoxyacetophenone

Guidance literature:: With hydrogenchloride; In acetic acid; for 1.41667h; Yield given; Ambient temperature;
DOI:10.1246/bcsj.56.3773

Reference yield:

: 21919-66-4
2,30dihydroxy-4,6-dimethoxyacetophenone

: 54299-57-9
3-benzyloxy-2-hydroxy-4,6-dimethoxyacetophenone

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / dimethylformamide / 3 h / Heating

2: conc.HCl / acetic acid / 1.42 h / Ambient temperature

With hydrogenchloride; potassium carbonate; In acetic acid; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.56.3773

Reference yield:

: 100-44-7
benzyl chloride

: 54299-57-9
3-benzyloxy-2-hydroxy-4,6-dimethoxyacetophenone

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / dimethylformamide / 3 h / Heating

2: conc.HCl / acetic acid / 1.42 h / Ambient temperature

With hydrogenchloride; potassium carbonate; In acetic acid; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.56.3773