2-Bromo-1-(4-methylphenyl)-3-phenylpropane-1,3-dione

Base Information

Chemical Name:2-Bromo-1-(4-methylphenyl)-3-phenylpropane-1,3-dione
CAS No.:54458-30-9
Molecular Formula:C16H13BrO2
Molecular Weight:317.182
Hs Code.:
DSSTox Substance ID:DTXSID30520044

Synonyms:54458-30-9;2-Bromo-1-(4-methylphenyl)-3-phenylpropane-1,3-dione;1,3-Propanedione, 2-bromo-1-(4-methylphenyl)-3-phenyl-;2-Bromo-1-phenyl-3-p-tolylpropane-1,3-dione;DTXSID30520044

Suppliers and Price of 2-Bromo-1-(4-methylphenyl)-3-phenylpropane-1,3-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Bromo-1-(4-methylphenyl)-3-phenylpropane-1,3-dione

Chemical Property:

XLogP3:4.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:316.00989
Heavy Atom Count:19
Complexity:326

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=C(C=C1)C(=O)C(C(=O)C2=CC=CC=C2)Br

Technology Process of 2-Bromo-1-(4-methylphenyl)-3-phenylpropane-1,3-dione

There total 8 articles about 2-Bromo-1-(4-methylphenyl)-3-phenylpropane-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 25855-99-6
1-(4-methylphenyl)-3-phenyl-1,3-propanedione

: 54458-30-9
2-bromo-1-(4-methylphenyl)-3-phenyl-1,3-propanedione

Guidance literature:: With N-Bromosuccinimide; at 20 ℃; for 12h; regioselective reaction; Sealed tube;
DOI:10.1002/ejoc.201800994

Reference yield: 82.0%

: 88039-22-9
2-bromo-3-imino-1-phenyl-N,3-di-p-tolylprop-1-enamine

: 54458-30-9
2-bromo-1-(4-methylphenyl)-3-phenyl-1,3-propanedione

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; at 70 ℃; for 6h;

Reference yield:

: 10325-65-2
2,3-Dibromo-3-phenyl-1-p-tolyl-propan-1-one

: 54458-30-9
2-bromo-1-(4-methylphenyl)-3-phenyl-1,3-propanedione

Guidance literature:: Multi-step reaction with 2 steps

1: NaOMe / methanol

2: Br₂, Py

With pyridine; bromine; sodium methylate; In methanol;
DOI:10.1002/hlca.19740570736