Benzenamine, N,N-dibutyl-4-ethynyl-3-[[tris(1-methylethyl)silyl]ethynyl]-

Base Information Edit

Chemical Name:Benzenamine, N,N-dibutyl-4-ethynyl-3-[[tris(1-methylethyl)silyl]ethynyl]-
CAS No.:547735-44-4
Molecular Formula:C27H43NSi
Molecular Weight:409.731
Hs Code.:
DSSTox Substance ID:DTXSID90463589
Nikkaji Number:J2.029.805G
Wikidata:Q82288543
Mol file:547735-44-4.mol

Synonyms:547735-44-4;Benzenamine, N,N-dibutyl-4-ethynyl-3-[[tris(1-methylethyl)silyl]ethynyl]-;DTXSID90463589

Suppliers and Price of Benzenamine, N,N-dibutyl-4-ethynyl-3-[[tris(1-methylethyl)silyl]ethynyl]-

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Benzenamine, N,N-dibutyl-4-ethynyl-3-[[tris(1-methylethyl)silyl]ethynyl]- Edit

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:13
Exact Mass:409.316476910
Heavy Atom Count:29
Complexity:552

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCN(CCCC)C1=CC(=C(C=C1)C#C)C#C[Si](C(C)C)(C(C)C)C(C)C

Technology Process of Benzenamine, N,N-dibutyl-4-ethynyl-3-[[tris(1-methylethyl)silyl]ethynyl]-

There total 3 articles about Benzenamine, N,N-dibutyl-4-ethynyl-3-[[tris(1-methylethyl)silyl]ethynyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 834856-13-2
N,N-dibutyl-3-[(triisopropylsilyl)ethynyl]-4-[(trimethylsilyl)ethynyl]aniline

: 547735-44-4
N,N-dibutyl-4-ethynyl-3-[(triisopropylsilyl)ethynyl]aniline

Guidance literature:: With potassium carbonate; In tetrahydrofuran; methanol; at 20 ℃;
DOI:10.1021/ja044175a

Reference yield:

: 248276-94-0
N,N-dibutyl-4-iodo-3-[(triisopropylsilyl)ethynyl]aniline

: 547735-44-4
N,N-dibutyl-4-ethynyl-3-[(triisopropylsilyl)ethynyl]aniline

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / Pd(PPh₃)4; CuI; iPr₂NH / tetrahydrofuran / 12 h / 20 °C

2: 100 percent / K₂CO₃ / tetrahydrofuran; methanol / 20 °C

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; diisopropylamine; In tetrahydrofuran; methanol; 1: Sonogashira cross-coupling;
DOI:10.1021/ja044175a