Boranamine, 1-[4-(dimethylamino)phenyl]-N,N-bis(1-methylethyl)-

Base Information

• Chemical Name: Boranamine, 1-[4-(dimethylamino)phenyl]-N,N-bis(1-methylethyl)-
• CAS No.: 547768-66-1
• Molecular Formula: C14H25BN2
• Molecular Weight: 232.177
• DSSTox Substance ID: DTXSID50460534
• Wikidata: Q82284603

Synonyms:547768-66-1;Boranamine, 1-[4-(dimethylamino)phenyl]-N,N-bis(1-methylethyl)-;DTXSID50460534

Chemical Property of Boranamine, 1-[4-(dimethylamino)phenyl]-N,N-bis(1-methylethyl)-

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 5
• Exact Mass: 231.2032539
• Heavy Atom Count: 17
• Complexity: 200

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: [B](C1=CC=C(C=C1)N(C)C)N(C(C)C)C(C)C

Technology Process of Boranamine, 1-[4-(dimethylamino)phenyl]-N,N-bis(1-methylethyl)-

There total 5 articles about Boranamine, 1-[4-(dimethylamino)phenyl]-N,N-bis(1-methylethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

4-Iodo-N,N-dimethylaniline (698-70-4) + diisopropopylaminoborane (22092-92-8) → 4-Me2-C6H4BHN(iPr)2 (547768-66-1)

Guidance literature:

With triethylamine; bis-triphenylphosphine-palladium(II) chloride; In 1,4-dioxane; at 70 ℃; for 15h;

DOI:10.1039/b306874a

Reference yield: 95.0%

→ 4-Me2-C6H4BHN(iPr)2 (547768-66-1)

Guidance literature:

Reference yield:

4-bromo-N,N-dimethylaniline (586-77-6) + diisopropopylaminoborane (22092-92-8) → 4-Me2-C6H4BHN(iPr)2 (547768-66-1)

Guidance literature:

With triethylamine; palladium; In 1,4-dioxane; at 78 ℃; for 15h;

DOI:10.1039/b308664j

upstream raw materials:

4-Iodo-N,N-dimethylaniline

diisopropopylaminoborane

4-bromo-N,N-dimethylaniline

N,N-diisopropylamine-borane

Downstream raw materials:

tris(4-dimethylamino phenyl)boroxine

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