Technology Process of 2H-Azonin-2-one, octahydro-1-(phenylmethyl)-
There total 3 articles about 2H-Azonin-2-one, octahydro-1-(phenylmethyl)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
2-azacyclononanone;
With
sodium hydride;
In
tetrahydrofuran;
at 0 ℃;
for 1h;
benzyl bromide;
In
tetrahydrofuran;
at 20 ℃;
for 24h;
DOI:10.13005/ojc/350215
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: di(n-butyl)tin oxide / toluene / 16 h / Dean-Stark; Reflux
2.1: sodium hydride / tetrahydrofuran / 1 h / 0 °C
2.2: 24 h / 20 °C
With
sodium hydride; di(n-butyl)tin oxide;
In
tetrahydrofuran; toluene;
DOI:10.13005/ojc/350215
- Guidance literature:
-
Natrium-8-octanlactam, Benzylchlorid;
