5,8,11-Trioxa-2-azadocosanoic acid, 22-mercapto-, 11-[ethoxy(4-nitrophenoxy)phosphinyl]undecyl ester

Base Information

Chemical Name:5,8,11-Trioxa-2-azadocosanoic acid, 22-mercapto-, 11-[ethoxy(4-nitrophenoxy)phosphinyl]undecyl ester
CAS No.:548430-86-0
Molecular Formula:C37H67N2O10PS
Molecular Weight:762.986
Hs Code.:

Synonyms:

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Chemical Property of 5,8,11-Trioxa-2-azadocosanoic acid, 22-mercapto-, 11-[ethoxy(4-nitrophenoxy)phosphinyl]undecyl ester

Chemical Property:

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Technology Process of 5,8,11-Trioxa-2-azadocosanoic acid, 22-mercapto-, 11-[ethoxy(4-nitrophenoxy)phosphinyl]undecyl ester

There total 8 articles about 5,8,11-Trioxa-2-azadocosanoic acid, 22-mercapto-, 11-[ethoxy(4-nitrophenoxy)phosphinyl]undecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 548430-85-9
11-[2-(2-{2-[11-(pyridin-2-yldisulfanyl)undecyloxy]ethoxy}ethoxy)ethylcarbamoyloxy]undecylphosphonic acid ethyl ester 4-nitrophenyl ester

: 548430-86-0
[11-(2-{2-[2-(11-mercaptoundecyloxy)ethoxy]ethoxy}ethylcarbamoyloxy)undecyl]phosphonic acid ethyl ester 4-nitrophenyl ester

Guidance literature:: With triethylamine; diothiothreitol; In methanol; at 20 ℃; for 20h; Inert atmosphere;

Reference yield:

: 2635-84-9
p-nitrophenyl butyrate

: 548430-86-0
[11-(2-{2-[2-(11-mercaptoundecyloxy)ethoxy]ethoxy}ethylcarbamoyloxy)undecyl]phosphonic acid ethyl ester 4-nitrophenyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: Fusarium solani pisi cutinase; water; propyl-phosphonic acid ethyl ester-(4-nitro-phenyl ester) / aq. phosphate buffer; dimethyl sulfoxide / 20 °C / pH 7 / Inert atmosphere; Enzymatic reaction

2.1: oxalyl dichloride / dichloromethane / 8 h / 0 - 20 °C / Inert atmosphere

2.2: 10 h / 20 °C / Inert atmosphere

3.1: triethylamine / N,N-dimethyl-formamide / 66 h / 60 °C / Inert atmosphere

4.1: triethylamine; diothiothreitol / methanol / 20 h / 20 °C / Inert atmosphere

With oxalyl dichloride; propyl-phosphonic acid ethyl ester-(4-nitro-phenyl ester); water; triethylamine; diothiothreitol; Fusarium solani pisi cutinase; In methanol; aq. phosphate buffer; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: imidazole carboxylic acid (diethoxyphosphoryl)undecyl ester

: 548430-86-0
[11-(2-{2-[2-(11-mercaptoundecyloxy)ethoxy]ethoxy}ethylcarbamoyloxy)undecyl]phosphonic acid ethyl ester 4-nitrophenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: oxalyl dichloride / dichloromethane / 8 h / 0 - 20 °C / Inert atmosphere

1.2: 10 h / 20 °C / Inert atmosphere

2.1: triethylamine / N,N-dimethyl-formamide / 66 h / 60 °C / Inert atmosphere

3.1: triethylamine; diothiothreitol / methanol / 20 h / 20 °C / Inert atmosphere

With oxalyl dichloride; triethylamine; diothiothreitol; In methanol; dichloromethane; N,N-dimethyl-formamide;