3-Diazonio-1-methyl-4-oxoquinolin-2-olate

Base Information

Chemical Name:3-Diazonio-1-methyl-4-oxoquinolin-2-olate
CAS No.:41878-47-1
Molecular Formula:C10H7N3O2
Molecular Weight:201.184
Hs Code.:
DSSTox Substance ID:DTXSID20383044
Nikkaji Number:J1.021.127A
Wikidata:Q82174602
Mol file:41878-47-1.mol

Synonyms:3-diazonio-1-methyl-4-oxoquinolin-2-olate;41878-47-1;DTXSID20383044;1-Methyl-3-diazoquinoline-2,4(1H,3H)-dione;3-diazo-1-methyl-2,4(1H,3H)-quinolinedione;AE-406/41056653

Suppliers and Price of 3-Diazonio-1-methyl-4-oxoquinolin-2-olate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 0 raw suppliers

Chemical Property of 3-Diazonio-1-methyl-4-oxoquinolin-2-olate

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
PSA：73.21000
Density:g/cm³
LogP:2.16688
XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:0
Exact Mass:201.053826475
Heavy Atom Count:15
Complexity:379

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1C2=CC=CC=C2C(=O)C(=C1[O-])[N+]#N

Technology Process of 3-Diazonio-1-methyl-4-oxoquinolin-2-olate

There total 3 articles about 3-Diazonio-1-methyl-4-oxoquinolin-2-olate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 61469-95-2
1-methyl-1H-quinoline-2,4-dione

: 41878-47-1
3-diazo-1-methylquinoline-2,4(1H,3H)-dione

Guidance literature:: With sodium azide; 3-Carboxybenzenesulfonyl chloride; potassium carbonate; In water; acetonitrile; at 20 ℃; for 1.5h;
DOI:10.1039/c9cc02042j

Reference yield: 90.0%

: 1677-46-9
4-hydroxy-1-methyl-2(1H)-quinolone

: 41878-47-1
3-diazo-1-methylquinoline-2,4(1H,3H)-dione

Guidance literature:: With triethylamine; Methanesulfonyl azide; In ethanol; at 20 ℃; for 12h;
DOI:10.1021/jo982503h

Reference yield:

: 119-68-6
N-Methylanthranilic acid

: 41878-47-1
3-diazo-1-methylquinoline-2,4(1H,3H)-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / acetic acid / 5 h / Heating

2: 90 percent / mesyl azide; triethylamine / ethanol / 12 h / 20 °C

With triethylamine; Methanesulfonyl azide; In ethanol; acetic acid; 1: Cycloaddition / 2: Substitution;
DOI:10.1021/jo982503h